N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Base Information

Chemical Name:N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide
CAS No.:94094-49-2
Molecular Formula:C9H11 N O4 S
Molecular Weight:229.257
Hs Code.:2935009090
European Community (EC) Number:302-151-0
DSSTox Substance ID:DTXSID90916505
Nikkaji Number:J288.602B
Wikidata:Q82887748
Mol file:94094-49-2.mol

Synonyms:94094-49-2;N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide;5-METHANESULPHONAMIDO-2-HYDROXYACETOPHENONE;EINECS 302-151-0;N-(3-Acetyl-4-hydroxyphenyl)methanesulphonamide;SCHEMBL7355242;DTXSID90916505;AKOS037646029;AS-65938;FT-0766646

Suppliers and Price of N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-METHANESULPHONAMIDO-2-HYDROXYACETOPHENONE 95.00%
5MG
$ 505.68

Total 6 raw suppliers

Chemical Property of N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Chemical Property:

Vapor Pressure:9.18E-07mmHg at 25°C
Boiling Point:393.7°Cat760mmHg
Flash Point:191.9°C
PSA：91.85000
Density:1.433g/cm³
LogP:2.12010
XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:229.04087901
Heavy Atom Count:15
Complexity:333

Purity/Quality:

97% ^*data from raw suppliers

5-METHANESULPHONAMIDO-2-HYDROXYACETOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C=CC(=C1)NS(=O)(=O)C)O

Technology Process of N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

There total 6 articles about N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 57471-32-6
5-amino-2-hydroxyacetophenone hydrochloride

: 124-63-0
methanesulfonyl chloride

: 94094-49-2
N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 1h;
DOI:10.1021/jo00119a008

Reference yield: 69.0%

: 50-80-6
5-amino-2-hydroxyacetophenone

: 124-63-0
methanesulfonyl chloride

: 94094-49-2
N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1021/jm00099a028

Reference yield:

: 7298-67-1
5-acetamido-2-hydroxyacetophenone

: 94094-49-2
N-(3-acetyl-4-hydroxyphenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / aq. HCl

2: 69 percent / pyridine / CH₂Cl₂

With pyridine; hydrogenchloride; In dichloromethane;
DOI:10.1021/jm00099a028