RB 88724

Base Information

Chemical Name:RB 88724
CAS No.:145386-11-4
Molecular Formula:C₁₀H₁₀N₂O₅
Molecular Weight:238.2
Hs Code.:
Mol file:145386-11-4.mol

Synonyms:(+-)-3-(5-Nitro-2-furanyl)-N-(oxiranylmethyl)-2-propenamide;RB-88724;(E)-3-(5-nitro-2-furyl)-N-(oxiran-2-ylmethyl)prop-2-enamide;N-(2,3-Epoxypropyl)-3-(5-nitrofuran-2-yl)-propenamide;2-Propenamide, 3-(5-nitro-2-furanyl)-N-(oxiranylmethyl)-, (+-)-;

Suppliers and Price of RB 88724

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of RB 88724

Chemical Property:

Boiling Point:492.7°Cat760mmHg
Flash Point:251.8°C
Density:1.419g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of RB 88724

There total 4 articles about RB 88724 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 90915-90-5
3-(5-nitrofuran-2-yl)-N-(prop-2-enyl)propenamide

: 145386-11-4,129423-20-7
N-(oxiranylmethyl)-3-(5-nitrofuran-2-yl)propenamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2.5h; Heating;
DOI:10.1021/jm00171a027

Reference yield:

: 698-63-5
5-nitrofurane-2-carboxaldehyde

: 145386-11-4,129423-20-7
N-(oxiranylmethyl)-3-(5-nitrofuran-2-yl)propenamide

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / NaOAc / 2.5 h / 140 - 150 °C

2: SOCl₂, DMF / 3.5 h / Heating

3: 50 percent / Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

4: 47 percent / 3-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 2.5 h / Heating

With thionyl chloride; sodium acetate; triethylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00171a027

Reference yield:

: 7187-02-2
3(5-nitro-furan-2-yl)-acryloyl chloride

: 145386-11-4,129423-20-7
N-(oxiranylmethyl)-3-(5-nitrofuran-2-yl)propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

2: 47 percent / 3-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 2.5 h / Heating

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00171a027