1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-

Base Information

Chemical Name:1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-
CAS No.:63366-67-6
Molecular Formula:C₁₀H₂₀BN
Molecular Weight:165.087
Hs Code.:
DSSTox Substance ID:DTXSID20212764
Wikidata:Q83087961
Mol file:63366-67-6.mol

Synonyms:1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-;63366-67-6;1-Azabicyclo[3.3.1]nonane,1-dimethylboryl-;YVQRQNKJUCGEPO-UHFFFAOYSA-;DTXSID20212764;Methanamine,N-methyl-N-(9-boratabicyclo[3.3.1]non-9-yl);InChI=1/C10H20BN/c1-12(2)11-9-5-3-6-10(11)8-4-7-9/h9-10H,3-8H2,1-2H3

Suppliers and Price of 1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-

Chemical Property:

Vapor Pressure:0.0757mmHg at 25°C
Boiling Point:227.9°Cat760mmHg
Flash Point:91.6°C
PSA：3.24000
Density:0.88g/cm³
LogP:2.64770
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:165.1688798
Heavy Atom Count:12
Complexity:136

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(C2CCCC1CCC2)N(C)C

Technology Process of 1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl-

There total 9 articles about 1-Azabicyclo(3.3.1)nonane, 1-dimethylboryl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 21205-91-4
9-borabicyclo[3.3.1]nonane dimer

: 124-40-3
dimethyl amine

: 63366-67-6
9-(dimethylamino)-9-borabicyclo{3.3.1}nonane

Guidance literature:: In hexane; a stirred soln. of B-compd. was saturated with anhydrous dimethylamine, heated to reflux while a slow flow of amine was mantained, rapid gas evolution began at about 60°C, after 15 min soln. was clear, refluxed for further 30 min; solvent distilled under atm. pressure, residue distilled under reduced pressure;

Reference yield: 75.0%

: 14610-26-5
1-phenyl-2-bis(dimethylamino)borylethyne

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 167896-89-1
dimeric (dimethylamino)(phenylethynyl)borane

: 63366-67-6
9-(dimethylamino)-9-borabicyclo{3.3.1}nonane

Guidance literature:: In tetrahydrofuran; N2 atmosphere, addn. of soln. of 9-BBN-H to soln. of alkynylborane at room temp., stirring (14 h); removement of volatiles (vacuum), crystn. (pentane, -78°C), decantation, drying (vacuum), isolation of byproduct: distillation of solvent, condensation into a trap (-78°C) at 32°C (1E-2 Torr); elem. anal.;