Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]-

Base Information

Chemical Name:Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]-
CAS No.:67341-38-2
Molecular Formula:C37H48N4O8S4
Molecular Weight:805.074
Hs Code.:

Synonyms:1,5,9,13-tetra-(p-tolylsulfonyl)-1,5,9,13-tetraazatridecane;1,5,9,13-tetratosyl-1,5,9,13-tetraazatridecane;1,4,8,12-tetratisyl-1,4,8,12-tetrazadodecane;N,N',4,8-tetra(p-toluenesulfonyl)-4,8-diazaundecane-1,11-diamine;1,5,9,13-tetra(p-tolylsulfonyl)-1,5,9,13-tetrazatridecane;

Suppliers and Price of Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]-

Chemical Property:

PSA：200.62000
LogP:9.83410

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]-

There total 10 articles about Benzenesulfonamide, N,N'-1,3-propanediylbis[4-methyl-N-[3-[[(4-methylphenyl)sulfonyl]amino] propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4605-14-5
N,N'-bis-(3-aminopropyl)-1,3-propanediamine

: 98-59-9
p-toluenesulfonyl chloride

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; for 24h;
DOI:10.1039/c3dt51012c

Reference yield: 72.0%

: 87265-93-8
4,8-di(p-toluenesulfonyl)-4,8-diazaundecane-1,11-diamine

: 98-59-9
p-toluenesulfonyl chloride

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1002/hlca.19830660426

Reference yield:

: 53364-99-1
N,N'-ditoluenesulfonyl-1,3-diaminopropane

: 67341-38-2
N,N'-bis<3-(tosylamino)propyl>-N,N'-ditosyl-1,3-propanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Cs₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 92 percent / N₂H₄*H₂O / 23 h / 75 °C

3: 2M HCl / ethanol / 4 h / 80 °C

4: Et₃N, pyridine / 4 h / Ambient temperature

With pyridine; hydrogenchloride; caesium carbonate; hydrazine hydrate; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.62.198