Bis(p-nitrobenzyl) Phosphate

Base Information

• Chemical Name: Bis(p-nitrobenzyl) Phosphate
• CAS No.: 14390-40-0
• Molecular Formula: C14H13N2O8P
• Molecular Weight: 368.2354
• Mol file: 14390-40-0.mol

Synonyms:Bis[(4-nitrophenyl)methyl] hydrogen phosphate;

Chemical Property of Bis(p-nitrobenzyl) Phosphate

Chemical Property:

• Vapor Pressure: 2.19E-14mmHg at 25°C
• Melting Point: 173-174 °C
• Refractive Index: 1.625
• Boiling Point: 582 °C at 760 mmHg
• PKA: 1.25±0.50(Predicted)
• Flash Point: 305.8 °C
• PSA: 157.21000
• Density: 1.527 g/cm³
• LogP: 4.38320
• Storage Temp.: Refrigerator
• Solubility.: DMSO

Purity/Quality:

99% ^*data from raw suppliers

Bis(p-nitrobenzyl)Phosphate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Phosphorylating reagent

Technology Process of Bis(p-nitrobenzyl) Phosphate

There total 4 articles about Bis(p-nitrobenzyl) Phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosphoric acid tris-(4-nitro-benzyl ester) (66777-93-3) → phosphoric acid bis-(4-nitro-benzyl ester) (14390-40-0)

Guidance literature:

With acetone; sodium iodide;

DOI:10.1021/ja01625a045 DOI:10.1017/S1092852900007914

Reference yield:

4-nitrobenzyl chloride (619-73-8) → phosphoric acid bis-(4-nitro-benzyl ester) (14390-40-0)

Guidance literature:

With pyridine; methyl dichlorophosphoridate;

DOI:10.1016/0040-4020(75)80203-1

Reference yield:

4-methyl-morpholine (109-02-4) + phosphoric acid tris-(4-nitro-benzyl ester) (66777-93-3) → phosphoric acid bis-(4-nitro-benzyl ester) (14390-40-0)

Guidance literature:

Erwaermen auf dem Dampfbad und Behandeln des Reaktionsprodukts mit wss. HCl;

upstream raw materials:

4-methyl-morpholine

phosphoric acid tris-(4-nitro-benzyl ester)

4-nitrobenzyl chloride

Downstream raw materials:

Diphosphorsaeure-tetrakis-(4-nitro-benzylester)

chlorophosphoric acid bis-(4-nitro-benzyl ester)

diphosphoric acid-1,2-bis-(4-nitro-benzyl ester)

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