Tris(p-nitrobenzyl) Phosphate

Base Information

• Chemical Name: Tris(p-nitrobenzyl) Phosphate
• CAS No.: 66777-93-3
• Molecular Formula: C21H18 N3 O10 P
• Molecular Weight: 503.362
• Mol file: 66777-93-3.mol

Synonyms:NSC 401698;Tris(p-nitrobenzyl) phosphate

Chemical Property of Tris(p-nitrobenzyl) Phosphate

Chemical Property:

• Vapor Pressure: 3.79E-18mmHg at 25°C
• Melting Point: 127-128 °C
• Boiling Point: 690.8°Cat760mmHg
• Flash Point: 371.6°C
• PSA: 192.03000
• Density: 1.485g/cm³
• LogP: 7.03910
• Solubility.: DMSO

Purity/Quality:

99% ^*data from raw suppliers

Tris(p-nitrobenzyl)Phosphate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tris(p-nitrobenzyl) Phosphate

There total 2 articles about Tris(p-nitrobenzyl) Phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrobenzyl chloride (100-14-1) → phosphoric acid tris-(4-nitro-benzyl ester) (66777-93-3)

Guidance literature:

With silver orthophosphate; chloroform;

DOI:10.1021/ja01625a045

Reference yield:

1-bromomethyl-4-nitro-benzene (100-11-8) → phosphoric acid tris-(4-nitro-benzyl ester) (66777-93-3)

Guidance literature:

With silver orthophosphate; acetonitrile;

Reference yield:

phosphoric acid tris-(4-nitro-benzyl ester) (66777-93-3) → phosphoric acid (86119-84-8,7664-38-2) + p-toluidine (106-49-0,12221-03-3)

Guidance literature:

Hydrogenation;

upstream raw materials:

4-nitrobenzyl chloride

1-bromomethyl-4-nitro-benzene

Downstream raw materials:

phosphoric acid bis-(4-nitro-benzyl ester)

phosphoric acid

p-toluidine

chlorophosphoric acid bis-(4-nitro-benzyl ester)