Ethyl 2,4-dioxo-6-phenylhex-5-enoate

Base Information

Chemical Name:Ethyl 2,4-dioxo-6-phenylhex-5-enoate
CAS No.:1027-41-4
Molecular Formula:C14H14 O4
Molecular Weight:246.263
Hs Code.:
NSC Number:122409
Mol file:1027-41-4.mol

Synonyms:ethyl 2,4-dioxo-6-phenylhex-5-enoate;209455-68-5;1027-41-4;NSC122409;SCHEMBL7423204;SCHEMBL7423208;ZYTPZSVMXSYIFE-CMDGGOBGSA-N;NSC-122409;Ethyl (5E)-2,4-dioxo-6-phenyl-5-hexenoate #;5-Hexenoic acid, 2,4-dioxo-6-phenyl-, ethyl ester

Suppliers and Price of Ethyl 2,4-dioxo-6-phenylhex-5-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Ethyl 2,4-dioxo-6-phenylhex-5-enoate

Chemical Property:

Vapor Pressure:3E-06mmHg at 25°C
Boiling Point:388.7°Cat760mmHg
Flash Point:172.6°C
Density:1.168g/cm³
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:246.08920892
Heavy Atom Count:18
Complexity:338

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=O)CC(=O)C=CC1=CC=CC=C1
Isomeric SMILES:CCOC(=O)C(=O)CC(=O)/C=C/C1=CC=CC=C1

Technology Process of Ethyl 2,4-dioxo-6-phenylhex-5-enoate

There total 6 articles about Ethyl 2,4-dioxo-6-phenylhex-5-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 95-92-1
oxalic acid diethyl ester

: 1896-62-4
(E)-benzalacetone

: 1027-41-4
ethyl (E)-2,4-dioxo-6-phenylhex-5-enoate

Guidance literature:: With sodium ethanolate; In diethyl ether; at 20 ℃; for 16.5h;

Reference yield:

: 95-92-1
oxalic acid diethyl ester

: 122-57-6
1-Phenylbut-1-en-3-one

: 1027-41-4
ethyl (E)-2,4-dioxo-6-phenylhex-5-enoate

Guidance literature:: With sodium; at -5 - 20 ℃; for 16.5h;

Reference yield:

: 85763-14-0
(E)-2,4-Dioxo-6-phenyl-hex-5-enoic acid

: 1027-41-4
ethyl (E)-2,4-dioxo-6-phenylhex-5-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Ac₂O / 0.17 h / Heating

2: 65 percent / benzene

With acetic anhydride; In benzene;