(2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one

Base Information

Chemical Name:(2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one
CAS No.:124151-21-9
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:
Mol file:124151-21-9.mol

Synonyms:Cyclohexanone,2-[1-(3-furanyl)-2-nitropropyl]-, [2R*(1R*,2S*)]- (9CI); Cyclohexanone, 2-[1-(3-furanyl)-2-nitropropyl]-,[2R*(1R*,2S*)]-(?à)-

Suppliers and Price of (2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one

Chemical Property:

Vapor Pressure:2.68E-06mmHg at 25°C
Boiling Point:390.3°Cat760mmHg
Flash Point:189.8°C
Density:1.191g/cm³

Purity/Quality:

Safty Information:

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Technology Process of (2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one

There total 7 articles about (2R)-2-[(1R)-1-(3-furyl)-2-nitro-propyl]cyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 2981-10-4
1-(cyclohex-1-en-1-yl)piperidine

: 124070-88-8,860003-90-3
(E)-1-(3-furyl)-2-nitro-1-propene

: 124070-90-2,124151-19-5,124151-20-8,124151-21-9
(1'RS,2SR)-2-<1'-(3-furyl)-2'-nitropropyl>cyclohexanone

: 124070-90-2,124151-19-5,124151-20-8,124151-21-9
(1'RS,2SR)-2-<1'-(3-furyl)-2'-nitropropyl>cyclohexanone

Guidance literature:: In diethyl ether; for 21h; Ambient temperature;
DOI:10.1021/jo00291a048

Reference yield: 3.0%

: 2981-10-4
1-(cyclohex-1-en-1-yl)piperidine

: 124070-88-8,860003-90-3
(E)-1-(3-furyl)-2-nitro-1-propene

: 124070-90-2,124151-19-5,124151-20-8,124151-21-9
(1'RS,2SR)-2-<1'-(3-furyl)-2'-nitropropyl>cyclohexanone

: 124070-90-2,124151-19-5,124151-20-8,124151-21-9
(1'RS,2SR)-2-<1'-(3-furyl)-2'-nitropropyl>cyclohexanone

Guidance literature:: In diethyl ether; for 21h; Ambient temperature;
DOI:10.1021/jo00291a048

Reference yield:

: 124070-88-8,860003-90-3
(E)-1-(3-furyl)-2-nitro-1-propene

: 124070-90-2,124151-19-5,124151-20-8,124151-21-9
(1'RS,2SR)-2-<1'-(3-furyl)-2'-nitropropyl>cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 18.1 percent / (i-PrO)4Ti, TiCl₄ / CH₂Cl₂ / -90 deg C, 90 min

2: KF / methanol / 5 h / Ambient temperature

With titanium(IV) isopropylate; potassium fluoride; titanium tetrachloride; In methanol; dichloromethane;
DOI:10.1021/jo00291a048