1H-Inden-1-ol, 2,3-dihydro-7-(1-methylethyl)-

Base Information

Chemical Name:1H-Inden-1-ol, 2,3-dihydro-7-(1-methylethyl)-
CAS No.:676121-66-7
Molecular Formula:C12H16O
Molecular Weight:176.258
Hs Code.:

Synonyms:

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Chemical Property of 1H-Inden-1-ol, 2,3-dihydro-7-(1-methylethyl)-

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Technology Process of 1H-Inden-1-ol, 2,3-dihydro-7-(1-methylethyl)-

There total 1 articles about 1H-Inden-1-ol, 2,3-dihydro-7-(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65651-63-0,38836-21-4
4-hydroxy-5-methyl-hexan-2-one

: 676121-66-7
7-isopropylindan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 71 percent / p-TsOH*H₂O; Na₂SO₄ / benzene / 5 h / 90 °C

2: 79 percent / LiN(TMS)2 / tetrahydrofuran; toluene / 1.17 h / -78 - 20 °C

3: 2,5-di-tert-butylhydroquinone / benzene / 56 h / 200 °C

4: p-TsOH*H₂O / acetone / 0.5 h / 20 °C

5: 75 percent / p-cymene / Pd/C / 45 h / 200 °C

6: 97 percent / NaH / tetrahydrofuran / 2.5 h / 20 °C

7: 87 percent / NaBH₄; NiCl₂*6H₂O / methanol / 3 h / 0 - 20 °C

With sodium tetrahydroborate; 4-methylisopropylbenzene; 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; sodium hydride; toluene-4-sulfonic acid; sodium sulfate; nickel dichloride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; acetone; toluene; benzene; 3: Diels-Alder reaction;
DOI:10.1021/jo049381f

Reference yield:

: 676121-66-7
7-isopropylindan-1-ol

: 461641-15-6
5-isopropyl-4-phenyl-1,9,9a,10a-tetrahydro-4H,4bH-10-oxa-4a-aza-indeno[1,2-a]indene-2-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / pTsOH*H₂O / benzene / 0.67 h / 20 - 100 °C

2.1: 86 percent / mCPBA; Mn(III) complex of (S,S)-1,2-cyclohexanediamine derivative; N-methylmorpholine N-oxide / CH₂Cl₂ / 1 h / -78 °C

3.1: H₂SO₄; acetonitrile / hexane / 1 h / 20 °C

3.2: 39 percent / H₂O / 2 h / 100 °C

4.1: CHCl₃ / 3 h / 24 °C

With Mn(III) complex of (S,S)-1,2-cyclohexanediamine derivative; sulfuric acid; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; acetonitrile; In hexane; dichloromethane; chloroform; benzene; 2.1: Jacobsen reaction / 3.1: Ritter reaction;
DOI:10.1021/jo049381f

Reference yield:

: 676121-66-7
7-isopropylindan-1-ol

: 461641-20-3
(1S,2R)-(-)-cis-1-[(2R)-4-hydroxymethyl-2-phenyl-1,2,5,6-tetrahydropyridin-1-yl]-7-isopropylindan-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / pTsOH*H₂O / benzene / 0.67 h / 20 - 100 °C

2.1: 86 percent / mCPBA; Mn(III) complex of (S,S)-1,2-cyclohexanediamine derivative; N-methylmorpholine N-oxide / CH₂Cl₂ / 1 h / -78 °C

3.1: H₂SO₄; acetonitrile / hexane / 1 h / 20 °C

3.2: 39 percent / H₂O / 2 h / 100 °C

4.1: CHCl₃ / 3 h / 24 °C

5.1: 1.12 g / LiAlH₄ / diethyl ether; tetrahydrofuran / 0.08 h / 20 °C

With lithium aluminium tetrahydride; Mn(III) complex of (S,S)-1,2-cyclohexanediamine derivative; sulfuric acid; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; acetonitrile; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; chloroform; benzene; 2.1: Jacobsen reaction / 3.1: Ritter reaction;
DOI:10.1021/jo049381f