2,2,2-Trichloro-1,1-dimethylethyl chloroformate

Base Information

Chemical Name:2,2,2-Trichloro-1,1-dimethylethyl chloroformate
CAS No.:66270-36-8
Molecular Formula:C5H6Cl4O2
Molecular Weight:239.913
Hs Code.:2915900090
European Community (EC) Number:266-293-4
UNII:ND4GQH3PK3
DSSTox Substance ID:DTXSID10216473
Nikkaji Number:J286.753B
Wikidata:Q83092703

Synonyms:2,2,2-Trichloro-1,1-dimethylethyl chloroformate;66270-36-8;TCBoc-chloride;(1,1,1-trichloro-2-methylpropan-2-yl) carbonochloridate;ND4GQH3PK3;1,1,1-trichloro-2-methylpropan-2-yl carbonochloridate;2,2,2-trichloro-tert-butyl chloroformate;EINECS 266-293-4;UNII-ND4GQH3PK3;|A,|A,|A-Trichloro-tert-butyl chloroformate;C5H6Cl4O2;|A,|A,|A-Trichloro-tert-butoxycarbonyl chloride;SCHEMBL56282;DTXSID10216473;GMELMFSDPDSXOZ-UHFFFAOYSA-N;MFCD00000801;AKOS015913026;AS-76079;SY273473;NS00035992;D93168;A936992;beta,beta,beta-Trichloro-tert-butoxycarbonyl chloride;1,1,1-Trichloro-2-methyl-2-propyl Carbonochloridate;2,2,2-Trichloro-1,1-dimethylethyl chloroformate, 96%;2,2,2-TRICHLORO-1,1-DIMETHYLETHOXYCARBONYL CHLORIDE;2,2,2-TRICHLORO-1,1-DIMETHYLETHYL CARBONOCHLORIDATE

Suppliers and Price of 2,2,2-Trichloro-1,1-dimethylethyl chloroformate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2,2,2-Trichloro-1,1-dimethylethyl chloroformate 96%
25g
$ 275.00

Sigma-Aldrich
2,2,2-Trichloro-1,1-dimethylethyl chloroformate 96%
5g
$ 76.20

American Custom Chemicals Corporation
2,2,2-TRICHLORO-1,1-DIMETHYLETHYL CHLOROFORMATE 95.00%
25G
$ 1337.67

American Custom Chemicals Corporation
2,2,2-TRICHLORO-1,1-DIMETHYLETHYL CHLOROFORMATE 95.00%
5G
$ 856.81

Total 21 raw suppliers

Chemical Property of 2,2,2-Trichloro-1,1-dimethylethyl chloroformate

Chemical Property:

Vapor Pressure:0.407mmHg at 25°C
Melting Point:28-30oC(lit.)
Boiling Point:196°Cat760mmHg
Flash Point:86.1°C
PSA：26.30000
Density:1.497g/cm³
LogP:3.51060
Storage Temp.:2-8°C
Solubility.:ethanol: soluble10%, clear, colorless
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:239.909240
Heavy Atom Count:11
Complexity:160

Purity/Quality:

98% ^*data from raw suppliers

2,2,2-Trichloro-1,1-dimethylethyl chloroformate 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s): 1935464
Hazard Codes:T
Statements: 23/24/25-34
Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC(C)(C(Cl)(Cl)Cl)OC(=O)Cl

Technology Process of 2,2,2-Trichloro-1,1-dimethylethyl chloroformate

There total 4 articles about 2,2,2-Trichloro-1,1-dimethylethyl chloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 57-15-8
1,1,1-trichloro-2-methyl-2-propanol

: 66270-36-8
2,2,2-trichloro-1,1-dimethylethoxychloroformate

Guidance literature:: With pyridine; at 20 ℃; for 96h;

Reference yield: 5.0%

: 86964-74-1
3-((2R,3R,4R,5R)-3,4-Diacetoxy-5-trityloxymethyl-tetrahydro-furan-2-yl)-2,6-dioxo-3,6-dihydro-2H-pyrimidine-1-carboxylic acid 2,2,2-trichloro-1,1-dimethyl-ethyl ester

: 66270-36-8
2,2,2-trichloro-1,1-dimethylethoxychloroformate

Guidance literature:: With triethylammonium phosphinate; In pyridine; at 45 ℃; for 5h; Product distribution; further reagents, temperatures, times, N-acyl derivatives;
DOI:10.1246/cl.1983.1051