(E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate

Base Information

Chemical Name:(E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate
CAS No.:22802-00-2
Molecular Formula:C₁₂H₁₂N₂O₅
Molecular Weight:264.238
Hs Code.:
NSC Number:112979
DSSTox Substance ID:DTXSID40714230
Wikidata:Q82650998
Mol file:22802-00-2.mol

Synonyms:22802-00-2;DTXSID40714230;NSC112979;NSC-112979;4-(2-DIAZOACETYL)-2,6-DIMETHOXYPHENYL ACETATE;(E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate

Suppliers and Price of (E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:264.07462149
Heavy Atom Count:19
Complexity:378

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=C(C=C(C=C1OC)C(=O)C=[N+]=[N-])OC

Technology Process of (E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate

There total 4 articles about (E)-1-[4-(Acetyloxy)-3,5-dimethoxyphenyl]-2-diazonioethen-1-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39657-47-1
O-acetylsyringic acid chloride

: 22802-00-2
1-(4-acetoxy-3,5-dimethoxy-phenyl)-2-diazo-ethanone

Guidance literature:: With diazomethane; In diethyl ether; at -5 - 0 ℃;
DOI:10.1039/c3pp50305d

Reference yield:

: 6318-20-3
O-acetylsyringic acid

: 22802-00-2
1-(4-acetoxy-3,5-dimethoxy-phenyl)-2-diazo-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 8 h / 80 °C / Inert atmosphere

2: diazomethane / diethyl ether / -5 - 0 °C

With diazomethane; thionyl chloride; In diethyl ether;
DOI:10.1039/c3pp50305d