N-[chloro(phenyl)phosphoryl]adamantan-1-amine

Base Information

Chemical Name:N-[chloro(phenyl)phosphoryl]adamantan-1-amine
CAS No.:56252-44-9
Molecular Formula:C16H21ClNOP
Molecular Weight:309.7708
Hs Code.:
NSC Number:166860
DSSTox Substance ID:DTXSID20304698

Synonyms:NSC166860;56252-44-9;DTXSID20304698;NSC-166860

Suppliers and Price of N-[chloro(phenyl)phosphoryl]adamantan-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-[chloro(phenyl)phosphoryl]adamantan-1-amine

Chemical Property:

Vapor Pressure:3.5E-07mmHg at 25°C
Boiling Point:417.6°Cat760mmHg
Flash Point:206.4°C
Density:1.26g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:309.1049290
Heavy Atom Count:20
Complexity:391

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2CC3CC1CC(C2)(C3)NP(=O)(C4=CC=CC=C4)Cl

Technology Process of N-[chloro(phenyl)phosphoryl]adamantan-1-amine

There total 2 articles about N-[chloro(phenyl)phosphoryl]adamantan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 768-94-5
1-Adamantanamine

: 56252-44-9
N-(1-adamantyl)phenylphosphonochloramidate

Guidance literature:: With triethylamine; In diethyl ether; for 7h; Ambient temperature;
DOI:10.1080/10426509608037956

Reference yield:

: 56252-44-9
N-(1-adamantyl)phenylphosphonochloramidate

Guidance literature:: 1-Aminoadamantan, Cl2POPh;

Reference yield:

: 56252-44-9
N-(1-adamantyl)phenylphosphonochloramidate

: 61733-60-6
ethyl methyl phenylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) aq. NaOH, 2.) aq. HCl / 1.) acetone, room temperature, 1 h, 2.) acetone

2: 68.4 percent / ethanol; toluene / 0.5 h / 120 °C

3: diethyl ether

With hydrogenchloride; sodium hydroxide; In diethyl ether; ethanol; toluene;
DOI:10.1080/10426509608037956