1-(1-Hydroxynaphthalen-2-yl)heptan-1-one

Base Information

Chemical Name:1-(1-Hydroxynaphthalen-2-yl)heptan-1-one
CAS No.:67013-66-5
Molecular Formula:C17H20O2
Molecular Weight:256.3395
Hs Code.:
NSC Number:34949
DSSTox Substance ID:DTXSID60284026
Wikidata:Q82018819
ChEMBL ID:CHEMBL1996960

Synonyms:1-(1-hydroxynaphthalen-2-yl)heptan-1-one;67013-66-5;NSC34949;CHEMBL1996960;DTXSID60284026;NSC-34949;NCI60_003115

Suppliers and Price of 1-(1-Hydroxynaphthalen-2-yl)heptan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(1-Hydroxynaphthalen-2-yl)heptan-1-one

Chemical Property:

Vapor Pressure:6.3E-07mmHg at 25°C
Boiling Point:398.7°Cat760mmHg
Flash Point:170.2°C
Density:1.085g/cm³
XLogP3:5.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:256.146329876
Heavy Atom Count:19
Complexity:287

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCC(=O)C1=C(C2=CC=CC=C2C=C1)O

Technology Process of 1-(1-Hydroxynaphthalen-2-yl)heptan-1-one

There total 5 articles about 1-(1-Hydroxynaphthalen-2-yl)heptan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 876896-45-6
(benzotriazol-1-yl)(1-hydroxynaphthalen-2-yl)methanone

: 3761-92-0
n-hexylmagnesium bromide

: 67013-66-5
1-(1-hydroxy-2-naphthyl)heptan-1-one

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 5h;
DOI:10.1055/s-2007-990786

Reference yield: 53.0%

: 3634-67-1
trihexylsilyl chloride

: 26639-33-8
N,N-diethyl-1-hydroxy-2-naphthamide

: 67013-66-5
1-(1-hydroxy-2-naphthyl)heptan-1-one

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jacs.8b03302

Reference yield:

: 85630-39-3
1-naphthyl N,N-diethylcarbamate

: 67013-66-5
1-(1-hydroxy-2-naphthyl)heptan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: lithium diisopropyl amide / tetrahydrofuran; hexane / 16 h / -78 - 20 °C / Inert atmosphere

2: lithium diisopropyl amide / tetrahydrofuran; hexane / 16 h / 0 - 20 °C / Inert atmosphere

With lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/jacs.8b03302