Ethyl 4-(4-cyanoanilino)benzoate

Base Information

Chemical Name:Ethyl 4-(4-cyanoanilino)benzoate
CAS No.:680983-41-9
Molecular Formula:C16H14N2O2
Molecular Weight:266.299
Hs Code.:
DSSTox Substance ID:DTXSID90457009
Wikidata:Q82279674

Synonyms:Ethyl 4-(4-cyanoanilino)benzoate;680983-41-9;SCHEMBL5472654;DTXSID90457009;FT-0737507

Suppliers and Price of Ethyl 4-(4-cyanoanilino)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethyl 4-(4-cyanoanilino)benzoate

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:266.105527694
Heavy Atom Count:20
Complexity:358

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC=C(C=C1)NC2=CC=C(C=C2)C#N

Technology Process of Ethyl 4-(4-cyanoanilino)benzoate

There total 8 articles about Ethyl 4-(4-cyanoanilino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 623-00-7
4-bromobenzenecarbonitrile

: 105230-46-4
4-carbethoxyphenyl-4-tolylazo sulfone

: 680983-41-9
ethyl 4-[(4-cyanophenyl)amino]-benzoate

Guidance literature:: Multistep reaction;
DOI:10.1002/anie.200603089

Reference yield:

: C₂₆H₂₅N₃O₄S

: 680983-41-9
ethyl 4-[(4-cyanophenyl)amino]-benzoate

Guidance literature:: With acetic acid; trifluoroacetic acid; zinc; at 75 ℃; for 2h;
DOI:10.1002/anie.200353241

Reference yield:

: 111017-08-4
ethyl 4-[bis(trimethylsilyl)amino]benzoate

: 680983-41-9
ethyl 4-[(4-cyanophenyl)amino]-benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 139 mg / aq. HCl / diethyl ether / 20 °C

2.1: HBF₄; NaNO₂ / H₂O / cooling

2.2: 71 percent / CH₂Cl₂ / 20 °C

With hydrogenchloride; tetrafluoroboric acid; sodium nitrite; In diethyl ether; water;
DOI:10.1002/anie.200603089