Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-

Base Information

Chemical Name:Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-
CAS No.:78613-00-0
Molecular Formula:C₂₀H₁₆Cl₂N₂O₃
Molecular Weight:403.265
Hs Code.:
DSSTox Substance ID:DTXSID10229205
Nikkaji Number:J92.917D
Wikidata:Q83109415
Mol file:78613-00-0.mol

Synonyms:78613-00-0;Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-;4-Acetyl-3-(2'-hydroxyethoxy)-5,6-bis(4-chlorophenyl)pyridazine;DTXSID10229205;LS-66392;2-[[4-Acetyl-5,6-bis(p-chlorophenyl)pyridazin-3-yl]oxy]ethanol

Suppliers and Price of Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-

Chemical Property:

Vapor Pressure:1.29E-15mmHg at 25°C
Boiling Point:607.6°Cat760mmHg
Flash Point:321.2°C
PSA：72.31000
Density:1.344g/cm³
LogP:4.69110
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:402.0537978
Heavy Atom Count:27
Complexity:480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=C(C(=NN=C1OCCO)C2=CC=C(C=C2)Cl)C3=CC=C(C=C3)Cl

Technology Process of Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)-

There total 3 articles about Ethanol, 2-((4-acetyl-5,6-bis(p-chlorophenyl)-3-pyridazinyl)oxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 107-21-1
ethylene glycol

: 78613-01-1
4-acetyl-3-chloro-5,6-bis(4-chlorophenyl)pyridazine

: 78613-00-0
4-acetyl-3-(2'-hydroxyethoxy)-5,6-bis(4-chlorophenyl)pyridazine

Guidance literature:: With potassium carbonate; In 1,4-dioxane; for 13h; Heating;
DOI:10.1002/jps.2600700419

Reference yield:

: 40036-75-7
(E)-4,4'-dichlorobenzil monohydrazone

: 78613-00-0
4-acetyl-3-(2'-hydroxyethoxy)-5,6-bis(4-chlorophenyl)pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / xylene / 7 h / 110 - 136 °C

2: 67 percent / POCl₃, Et₃N / 2 h / Heating

3: 68 percent / potassium carbonate / dioxane / 13 h / Heating

With pyridine; potassium carbonate; triethylamine; trichlorophosphate; In 1,4-dioxane; xylene;
DOI:10.1002/jps.2600700419

Reference yield:

: 75643-31-1
4-Acetyl-5,6-bis(p-chlorophenyl)-2H-pyridazin-3-one

: 78613-00-0
4-acetyl-3-(2'-hydroxyethoxy)-5,6-bis(4-chlorophenyl)pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / POCl₃, Et₃N / 2 h / Heating

2: 68 percent / potassium carbonate / dioxane / 13 h / Heating

With potassium carbonate; triethylamine; trichlorophosphate; In 1,4-dioxane;
DOI:10.1002/jps.2600700419