4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine

Base Information

Chemical Name:4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine
CAS No.:83548-60-1
Molecular Formula:C14H11 Cl N2 S
Molecular Weight:274.77
Hs Code.:2934999090
DSSTox Substance ID:DTXSID30406975
Wikidata:Q82212153
Mol file:83548-60-1.mol

Synonyms:4-chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine;83548-60-1;DTXSID30406975;2-Cyanopropan-2-yl-benzodithioate;AKOS002433739;CS-0225890;EN300-12515;Z119989986

Suppliers and Price of 4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-CHLORO-5,6-DIMETHYL-2-PHENYLTHIENO[2,3-D]PYRIMIDINE 95.00%
2.5G
$ 902.00

American Custom Chemicals Corporation
4-CHLORO-5,6-DIMETHYL-2-PHENYLTHIENO[2,3-D]PYRIMIDINE 95.00%
1G
$ 656.00

AK Scientific
4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine
250mg
$ 213.00

AK Scientific
4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine
100mg
$ 181.00

A2B
4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine 95%
1g
$ 302.00

Total 4 raw suppliers

Chemical Property of 4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine

Chemical Property:

Vapor Pressure:0.000166mmHg at 25°C
Boiling Point:340.8°C at 760 mmHg
Flash Point:159.9°C
PSA：54.02000
Density:1.313g/cm³
LogP:4.62850
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:274.0331472
Heavy Atom Count:18
Complexity:296

Purity/Quality:

99% ^*data from raw suppliers

4-CHLORO-5,6-DIMETHYL-2-PHENYLTHIENO[2,3-D]PYRIMIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(SC2=C1C(=NC(=N2)C3=CC=CC=C3)Cl)C

Technology Process of 4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine

There total 5 articles about 4-Chloro-5,6-dimethyl-2-phenylthieno[2,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4815-24-1
2-amino-4,5-dimethyl-3-thiophenecarboxylic acid ethyl ester

: 83548-60-1
4-Chloro-5,6-dimethyl-2-phenyl-thieno[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane / 3 h

2: POCl₃ / dioxane / 3 h / Heating

With hydrogenchloride; trichlorophosphate; In 1,4-dioxane;

Reference yield:

: 2227-79-4
benzenecarbothioamide

: 83548-60-1
4-Chloro-5,6-dimethyl-2-phenyl-thieno[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / Microwave irradiation

2: trichlorophosphate / Reflux

With trichlorophosphate; In neat (no solvent);
DOI:10.1039/c4ob00175c

Reference yield:

: 2-amino-3-carbethoxy-4,5-dimethylthiophene hydrochloride

: 83548-60-1
4-Chloro-5,6-dimethyl-2-phenyl-thieno[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / Microwave irradiation

2: trichlorophosphate / Reflux

With trichlorophosphate; In neat (no solvent);
DOI:10.1039/c4ob00175c