Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]-

Base Information

Chemical Name:Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]-
CAS No.:685886-67-3
Molecular Formula:C10H15BO5
Molecular Weight:226.037
Hs Code.:

Synonyms:2,6-dimethoxy-4-(methoxymethyl)phenylboric acid;2,6-dimethoxy-4-(methoxymethyl)phenylboronic acid;

Suppliers and Price of Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]-

Chemical Property:

PSA：68.15000
LogP:-0.47000

Purity/Quality:

Safty Information:

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Technology Process of Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]-

There total 4 articles about Boronic acid, [2,6-dimethoxy-4-(methoxymethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.8%

: 685886-78-6
2-bromo-1,3-dimethoxy-5-(methoxymethyl)benzene

: 121-43-7,63156-11-6
Trimethyl borate

: 685886-67-3
[2,6-dimethoxy-4-(methoxymethyl)phenyl]boronic acid

Guidance literature:: 2-bromo-1,3-dimethoxy-5-(methoxymethyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; for 0.5h; Cooling with acetone-dry ice;

Trimethyl borate; In tetrahydrofuran; hexane; at 0 ℃;

With hydrogenchloride; water; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.5h; Product distribution / selectivity;

Reference yield:

: 73569-69-4
1-methylmethoxy-3,5-dimethoxybenzene

: 685886-67-3
[2,6-dimethoxy-4-(methoxymethyl)phenyl]boronic acid

Guidance literature:: 1-methylmethoxy-3,5-dimethoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

With Triisopropyl borate; at -78 - 20 ℃;

Reference yield:

: 61367-62-2
(4-bromo-3,5-dimethoxyphenyl)methanol

: 685886-67-3
[2,6-dimethoxy-4-(methoxymethyl)phenyl]boronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / 1,2-dimethoxyethane / 0.5 h / 0 °C

1.2: 3 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h

2.2: 0 °C

2.3: 0.5 h / 20 °C

With n-butyllithium; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; hexane;