2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone

Base Information

Chemical Name:2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone
CAS No.:113458-65-4
Molecular Formula:C18H16 N8 O6
Molecular Weight:440.3696
Hs Code.:
Mol file:113458-65-4.mol

2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone

Synonyms:BRN 5679988;2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone;113458-65-4;C18H16N8O6;C18-H16-N8-O6;LS-70094

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.69g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:4
Exact Mass:440.11928026
Heavy Atom Count:32
Complexity:879

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=NNC(=O)NC2(C(=O)N(C1=O)C)C3=CC=C(C=C3)NN=CC4=CC=C(O4)[N+](=O)[O-]
Isomeric SMILES:CN1C2=NNC(=O)NC2(C(=O)N(C1=O)C)C3=CC=C(C=C3)N/N=C/C4=CC=C(O4)[N+](=O)[O-]

Technology Process of 2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone

There total 5 articles about 2-Furancarboxaldehyde, 5-nitro-, (4-(3,4,5,6,7,8-hexahydro-6,8-dimethyl-3,5,7-trioxopyrimido(5,4-e)-1,2,4-triazin-4a(2H)-yl)phenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 698-63-5
5-nitrofurane-2-carboxaldehyde

: 113458-64-3
2,3,4,4a,5,6,7,8-Octahydro-4a-(p-hydrazinophenyl)-6,8-dimethylpyrimido<5,4-e><1,2,4>triazine-3,5,7-trione

: 113458-65-4
2,3,4,4a,5,6,7,8-Octahydro-4a-<(5-nitrofurylmethylidene)-p-hydrazinophenyl>-6,8-dimethylpyrimido<5,4-e><1,2,4>triazine-3,5,7-trione

Guidance literature:: With hydrogenchloride; In ethanol; for 0.0833333h; Heating;
DOI:10.1007/BF00758763

Reference yield: 95.0%

: 18969-83-0
2,3,5,6,7,8-hexahydro-6,8-dimethylpyrimido<5,4-e>(1,2,4)-triazine-3,5,7-trione

: 726-50-1
1-(5-nitrofuran-2-ylmethylene)-2-phenylhydrazine

: 113458-65-4
2,3,4,4a,5,6,7,8-Octahydro-4a-<(5-nitrofurylmethylidene)-p-hydrazinophenyl>-6,8-dimethylpyrimido<5,4-e><1,2,4>triazine-3,5,7-trione

Guidance literature:: In ethanol; for 1h; Heating;
DOI:10.1007/BF00758763

Reference yield:

: 113458-69-8
2,3,4,4a,5,6,7,8-Octahydro-4a-ethoxy-6,8-dimethylpyrimido<5,4-e><1,2,4>triazine-3,5,7-trione

: 113458-65-4
2,3,4,4a,5,6,7,8-Octahydro-4a-<(5-nitrofurylmethylidene)-p-hydrazinophenyl>-6,8-dimethylpyrimido<5,4-e><1,2,4>triazine-3,5,7-trione

Guidance literature:: Multi-step reaction with 2 steps

1: P₂O₅ / 4 h / 150 - 155 °C

2: 95 percent / ethanol / 1 h / Heating

With phosphorus pentoxide; In ethanol;
DOI:10.1007/BF00758763