Methanone, [4-(hydroxymethyl)phenyl](6-methoxy-1H-indazol-3-yl)-

Base Information

Chemical Name:Methanone, [4-(hydroxymethyl)phenyl](6-methoxy-1H-indazol-3-yl)-
CAS No.:691905-46-1
Molecular Formula:C16H14N2O3
Molecular Weight:282.299
Hs Code.:

Synonyms:

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Chemical Property of Methanone, [4-(hydroxymethyl)phenyl](6-methoxy-1H-indazol-3-yl)-

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Technology Process of Methanone, [4-(hydroxymethyl)phenyl](6-methoxy-1H-indazol-3-yl)-

There total 7 articles about Methanone, [4-(hydroxymethyl)phenyl](6-methoxy-1H-indazol-3-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848468-06-4
C₂₇H₃₆N₂O₅Si

: 691905-46-1
C₁₆H₁₄N₂O₃

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 ℃; for 1h; celite;

Reference yield:

: 74457-86-6
1-(2-fluoro-4-methoxyphenyl)-1-ethanone

: 691905-46-1
C₁₆H₁₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrazine / ethylene glycol / 52 h / 20 - 150 °C

2.1: triethylamine / dmap / acetonitrile / 2 h / -5 - 20 °C

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 5 h / Heating / reflux; sun lamp

4.1: trimethylamine-N-oxide / dimethyl sulfoxide / 0.5 h / 0 °C

5.1: isopropylmagnesium chloride / 2 h / 20 °C

5.2: 2 h / 20 °C

6.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

7.1: hydrogenchloride / methanol / 1 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; trimethylamine-N-oxide; isopropylmagnesium chloride; triethylamine; pyridinium chlorochromate; hydrazine; dibenzoyl peroxide; dmap; In methanol; tetrachloromethane; dichloromethane; ethylene glycol; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 7746-29-4
6-methoxy-3-methyl-1H-indazole

: 691905-46-1
C₁₆H₁₄N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dmap / acetonitrile / 2 h / -5 - 20 °C

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 5 h / Heating / reflux; sun lamp

3.1: trimethylamine-N-oxide / dimethyl sulfoxide / 0.5 h / 0 °C

4.1: isopropylmagnesium chloride / 2 h / 20 °C

4.2: 2 h / 20 °C

5.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

6.1: hydrogenchloride / methanol / 1 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; trimethylamine-N-oxide; isopropylmagnesium chloride; triethylamine; pyridinium chlorochromate; dibenzoyl peroxide; dmap; In methanol; tetrachloromethane; dichloromethane; dimethyl sulfoxide; acetonitrile;