2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid

Base Information

Chemical Name:2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid
CAS No.:69438-62-6
Molecular Formula:C₁₀H₈Br₂O₂
Molecular Weight:319.98
Hs Code.:
DSSTox Substance ID:DTXSID90499424
Nikkaji Number:J1.037.334D

Synonyms:69438-62-6;2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid;DTXSID90499424

Suppliers and Price of 2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:319.88706
Heavy Atom Count:14
Complexity:259

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(C1(Br)Br)(C2=CC=CC=C2)C(=O)O

Technology Process of 2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid

There total 3 articles about 2,2-Dibromo-1-phenylcyclopropane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 156020-82-5
2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

: 69438-62-6,90314-20-8,90314-22-0
acide phenyl-1 dibromo-2,2 cyclopropane carboxylique

Guidance literature:: With formic acid; In water; for 3h; Heating;

Reference yield:

: 80234-04-4
2-phenylacrylaldehyde diethyl acetal

: 69438-62-6,90314-20-8,90314-22-0
acide phenyl-1 dibromo-2,2 cyclopropane carboxylique

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 50 percent aq. sodium hydroxide / 2.) TEBA / 1.) water

2: 97 percent / 80 percent formic acid / H₂O / 3 h / Heating

With sodium hydroxide; formic acid; N-benzyl-N,N,N-triethylammonium chloride; In water;