2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

Base Information

Chemical Name:2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal
CAS No.:156020-82-5
Molecular Formula:C₁₄H₁₈Br₂O₂
Molecular Weight:378.104
Hs Code.:

Synonyms:2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

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Chemical Property of 2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

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Technology Process of 2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

There total 1 articles about 2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-25-2
Bromoform

: 80234-04-4
2-phenylacrylaldehyde diethyl acetal

: 156020-82-5
2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Yield given. Multistep reaction; 1.) water;

Reference yield: 97.0%

: 156020-82-5
2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

: 69438-62-6,90314-20-8,90314-22-0
acide phenyl-1 dibromo-2,2 cyclopropane carboxylique

Guidance literature:: With formic acid; In water; for 3h; Heating;

Reference yield:

: 156020-82-5
2,2-dibromo-1-phenylcyclopropanecarbaldehyde diethylacetal

: 90314-24-2,90314-25-3,90314-26-4,90341-52-9,93590-95-5,143722-63-8
trans-2-bromo-1-phenylcyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 80 percent formic acid / H₂O / 3 h / Heating

2: 1.) MeLi, lithium bromide; 2.) 1.0 M HCl / 1.) 0 deg C, ether, petroleum ether, tetrahydrofuran, 1.5 h

With hydrogenchloride; formic acid; methyllithium; lithium bromide; In water;