1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE

Base Information

Chemical Name:1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE
CAS No.:69511-77-9
Molecular Formula:C16H15NO5
Molecular Weight:301.29400
Hs Code.:2914700090
Mol file:69511-77-9.mol

Synonyms:ursolic acid benzyl ester;Benzyl ursolate;Benzyl-4,5-dimethoxy-2-nitrophenylketon;

Suppliers and Price of 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE 95.00%
5MG
$ 503.34

Total 1 raw suppliers

Chemical Property of 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE

Chemical Property:

Melting Point:166-167 °C(Solv: ethanol (64-17-5); acetone (67-64-1))
Boiling Point:488.1±40.0 °C(Predicted)
PSA：81.35000
Density:1.247±0.06 g/cm3(Predicted)
LogP:3.56060

Purity/Quality:: 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE

There total 6 articles about 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-2-PHENYL-ETHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3141-93-3
4',5'-dimethoxydeoxybenzoin

: 69511-77-9
1-(4,5-dimethoxy-2-nitrophenyl)-2-phenyl-1-ethanone

Guidance literature:: With nitric acid; In acetic acid; at 15 ℃; for 0.5h;

Reference yield: 15.0%

: 69511-74-6
3-(4,5-Dimethoxy-2-nitro-phenyl)-3-oxo-2-phenyl-propionaldehyde

: 69511-77-9
1-(4,5-dimethoxy-2-nitrophenyl)-2-phenyl-1-ethanone

Guidance literature:: With sodium acetate; In ethanol; Heating;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 69511-77-9
1-(4,5-dimethoxy-2-nitrophenyl)-2-phenyl-1-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / benzene / 2.5 h / 55 - 60 °C

2: 63 percent / HNO₃; AcOH / 0.5 h / 0 - 20 °C

With aluminium trichloride; nitric acid; acetic acid; In benzene; 1: Friedel-Crafts reaction;
DOI:10.1016/j.tet.2006.10.056