Propanoic acid, 3-cyclohexylidene-

Base Information

• Chemical Name: Propanoic acid, 3-cyclohexylidene-
• CAS No.: 701-98-4
• Molecular Formula: C9H14O2
• Molecular Weight: 154.209
• Mol file: 701-98-4.mol

Synonyms:β-Cyclohexyliden-propionsaeure;3-cyclohexylidenepropanoic acid;3-cyclohexylidene-propanoic acid;3-cyclohexylidene-propionic acid;3-Cyclohexyliden-propionsaeure;

Chemical Property of Propanoic acid, 3-cyclohexylidene-

Chemical Property:

• PSA: 37.30000
• LogP: 2.35160

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Propanoic acid, 3-cyclohexylidene-

There total 12 articles about Propanoic acid, 3-cyclohexylidene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

1-vinylcyclohexanol (1940-19-8) + carbon monoxide (201230-82-2) → β-cyclohexylidenepropionic acid (701-98-4)

Guidance literature:

With dmap; palladium diacetate; acetic anhydride; triethylamine; triphenylphosphine; at 60 ℃; for 48h; under 7500.75 Torr; Reagent/catalyst; Temperature; Autoclave; Inert atmosphere;

Reference yield:

(E)-3-cyclohexylprop-2-enoic acid (56453-86-2) → β-cyclohexylidenepropionic acid (701-98-4)

Guidance literature:

DOI:10.1039/jr9370001140

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + (2-bromoethylidene)cyclohexane (932-86-5) → β-cyclohexylidenepropionic acid (701-98-4) + 1-ethenylcyclohexane-1-carboxylic acid

Guidance literature:

With tetraethylammonium perchlorate; magnesium; In N,N-dimethyl-formamide; at -10 ℃; electrochemical reaction;

DOI:10.1016/0040-4039(95)00537-M

upstream raw materials:

4-cyclohexylidene-2-butanone

triethanolamine

malonic acid

cyclohexanecarbaldehyde

Downstream raw materials:

3-cyclohexylidene-propionic acid ethyl ester

cyclohexanepropionic acid

cyclohexanone

3-cyclohexylpropanamide