2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate

Base Information

Chemical Name:2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate
CAS No.:70873-50-6
Molecular Formula:C9H11NO4
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID60499951
Wikidata:Q82351218

Synonyms:70873-50-6;2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate;DTXSID60499951

Suppliers and Price of 2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:197.06880783
Heavy Atom Count:14
Complexity:297

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)OC(=O)COC(=O)C(=C)C#N

Technology Process of 2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate

There total 2 articles about 2-Oxo-2-[(propan-2-yl)oxy]ethyl 2-cyanoprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-48-6
isopropyl chloroacetate

: 70873-50-6
2-Cyano-acrylic acid isopropoxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) NaBr, polyethylene glycol-400 / 2.) CH₃CN, 80 deg C, 6 h

2: 1.) piperidine, acetic acid, HCl, H₂O, tricresyl phosphate, 2.) P₂O₅, 2,6-di-(tert-butyl)p-cresol / 1.) cyclohexane, reflux, 1 h, 2.) 170-211 deg C, 0.5-1.0 mm Hg

With piperidine; hydrogenchloride; polyethylene glycol-400; phosphoric acid triphenyl ester; 2,6-di-tert-butyl-4-methyl-phenol; water; phosphorus pentoxide; acetic acid; sodium bromide;
DOI:10.1080/00304949809355288