2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde

Base Information

Chemical Name:2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde
CAS No.:71804-46-1
Molecular Formula:C12H14O4
Molecular Weight:222.241
Hs Code.:
DSSTox Substance ID:DTXSID10501134
Wikidata:Q82353294

Synonyms:71804-46-1;2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde;SCHEMBL25342040;DTXSID10501134

Suppliers and Price of 2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:222.08920892
Heavy Atom Count:16
Complexity:227

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=C(C(=C1OC)C=O)C)OC)C=O

Technology Process of 2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde

There total 6 articles about 2,5-Dimethoxy-3,6-dimethylbenzene-1,4-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 95306-71-1
1,4-di(bromomethyl)-2,5-dimethoxy-3,6-dimethylbenzene

: 71804-46-1
3,6-dimethoxy-2,5-dimethylterephtaldicarboxaldehyde

Guidance literature:: With dipotassium hydrogenphosphate; Potassium benzeneselenite; dibenzo-18-crown-6; In acetonitrile; for 30h;
DOI:10.1055/s-1984-30956

Reference yield: 90.0%

: 17228-83-0
2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

: 71804-46-1
3,6-dimethoxy-2,5-dimethylterephtaldicarboxaldehyde

Guidance literature:: With dipotassium hydrogenphosphate; 18-crown-6 ether; Potassium benzeneselenite; for 24h; Heating;
DOI:10.1016/S0040-4020(01)91854-X

Reference yield:

: 52954-54-8
1,4-dibromo-2,5-dimethoxy-3,6-dimethylbenzene

: 71804-46-1
3,6-dimethoxy-2,5-dimethylterephtaldicarboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: (i) nBuLi, Et₂O, (ii) /BRN= 1900390/

2: K₂CO₃ / acetone

3: iBu₂AlH / benzene

4: MnO₂ / diethyl ether

With manganese(IV) oxide; diisobutylaluminium hydride; potassium carbonate; In diethyl ether; acetone; benzene;