2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

Base Information

• Chemical Name: 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether
• CAS No.: 17228-83-0
• Molecular Formula: C₁₂H₁₆Cl₂O₂
• Molecular Weight: 263.164
• Mol file: 17228-83-0.mol

Synonyms:2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

Chemical Property of 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

There total 4 articles about 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,4-dimethoxy-2,5-dimethylbenzene (2674-32-0) + chloromethyl methyl ether (107-30-2) → 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether (17228-83-0)

Guidance literature:

With zinc(II) chloride; for 3.33333h; Ambient temperature;

DOI:10.1016/S0040-4020(01)91854-X

Reference yield: 80.0%

1,4-dimethoxy-2,5-dimethylbenzene (2674-32-0) → 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether (17228-83-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 70 ℃; for 5h;

DOI:10.1246/bcsj.53.2943

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,4-dimethoxy-2,5-dimethylbenzene (2674-32-0) → 2,5-dimethyl-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether (17228-83-0)

Guidance literature:

With hydrogenchloride; Durchleiten von HCl;

DOI:10.1021/ja01249a025

upstream raw materials:

formaldehyd

1,4-dimethoxy-2,5-dimethylbenzene

chloromethyl methyl ether

Downstream raw materials:

(2,5-dimethoxy-3,6-dimethyl-p-phenylene)-di-acetonitrile

3,6-dimethoxy-2,5-dimethylterephtaldicarboxaldehyde

2,5-bis(bromomethyl)-3,6-bis(chloromethyl)-p-hydroquinone dimethyl ether

5-[2,5-Bis-chloromethyl-3,6-dimethoxy-4-(4-methoxycarbonyl-3-oxo-butyl)-phenyl]-3-oxo-pentanoic acid methyl ester