Benzenesulfonamide, N-(4-bromophenyl)-N-methyl-

Base Information

• Chemical Name: Benzenesulfonamide, N-(4-bromophenyl)-N-methyl-
• CAS No.: 72385-31-0
• Molecular Formula: C13H12BrNO2S
• Molecular Weight: 326.214
• Hs Code.: 2935009090
• Mol file: 72385-31-0.mol

Synonyms:N-(4-bromophenyl)-N-methyl benzenesulfonamide;N-(4-bromophenyl)-N-methylbenzene-sulfonamide;4'-BROMO-N-METHYLBENZENESULFONANILIDE;

Chemical Property of Benzenesulfonamide, N-(4-bromophenyl)-N-methyl-

Chemical Property:

• PSA: 45.76000
• LogP: 4.35500

Purity/Quality:

4'-BROMO-N-METHYLBENZENESULFONANILIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, N-(4-bromophenyl)-N-methyl-

There total 6 articles about Benzenesulfonamide, N-(4-bromophenyl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-bromo-N,N-dimethylaniline (586-77-6) + benzenesulfonyl chloride (98-09-9) → N-(4-bromophenyl)-N-methyl-benzenesulfonamide (72385-31-0)

Guidance literature:

With cadmium sulphide; In ethanol; water; at 25 - 28 ℃; for 0.25h; Irradiation;

DOI:10.1021/acs.joc.0c02263

Reference yield: 85.0%

N-(4-bromophenyl)benzenesulfonamide (16468-97-6) + methyl iodide (74-88-4) → N-(4-bromophenyl)-N-methyl-benzenesulfonamide (72385-31-0)

Guidance literature:

N-(4-bromophenyl)benzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1016/j.bmc.2018.07.038

Reference yield:

4-bromo-N-methylaniline (6911-87-1,211060-12-7) → N-(4-bromophenyl)-N-methyl-benzenesulfonamide (72385-31-0)

Guidance literature:

With benzenesulfonyl chloride; In pyridine;

upstream raw materials:

N-(4-bromophenyl)benzenesulfonamide

methyl iodide

4-bromo-N-methylaniline

benzenesulfonyl chloride

Downstream raw materials:

N-[4-(Hydroxy-pyridin-3-yl-methyl)-phenyl]-N-methyl-benzenesulfonamide

C₂₂H₂₃F₃N₂O₃S

C₂₁H₂₁F₃N₂O₃S

C₂₀H₁₉F₃N₂O₃S