Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester

Base Information

Chemical Name:Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester
CAS No.:72668-64-5
Molecular Formula:C13H16O5
Molecular Weight:252.267
Hs Code.:
DSSTox Substance ID:DTXSID30459148
Wikidata:Q82282793

Synonyms:72668-64-5;Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester;DTXSID30459148

Suppliers and Price of Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:252.09977361
Heavy Atom Count:18
Complexity:254

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)COC1=CC=C(C=C1)C2OCCO2

Technology Process of Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester

There total 2 articles about Acetic acid, [4-(1,3-dioxolan-2-yl)phenoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 72668-64-5
ethyl [4-(1,3-dioxolan-2-yl)phenoxy]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 3 h / Heating

2: TsOH / benzene / 5 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In acetone; benzene;
DOI:10.1021/jo035052w

Reference yield:

: 51264-69-8
ethyl 2-(4-formylphenoxy)acetate

: 107-21-1
ethylene glycol

: 72668-64-5
ethyl [4-(1,3-dioxolan-2-yl)phenoxy]acetate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 5h; Heating;
DOI:10.1021/jo035052w

Reference yield: 38.0%

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 72668-64-5
ethyl [4-(1,3-dioxolan-2-yl)phenoxy]acetate

: (+/-)-(2R,3S)-ethyl 2-[4-(1,3-dioxolan-2-yl)phenoxy]-3-hydroxy-3-(3,4-dimethoxyphenyl)propionate

: (+/-)-(2S,3S)-ethyl 2-[4-(1,3-dioxolan-2-yl)phenoxy]-3-hydroxy-3-(3,4-dimethoxyphenyl)propionate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 0.833333h;
DOI:10.1021/jo035052w