6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine

Base Information

Chemical Name:6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine
CAS No.:7331-80-8
Molecular Formula:C₁₄H₁₁Br₂NO
Molecular Weight:369.055
Hs Code.:
DSSTox Substance ID:DTXSID60365748
Nikkaji Number:J485.785B
Wikidata:Q82150677
Mol file:7331-80-8.mol

Synonyms:7331-80-8;6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine;DTXSID60365748;STK793181;AKOS005611870;3,4-Dihydro-3-(4-bromophenyl)-6-bromo-2H-1,3-benzoxazine

Suppliers and Price of 6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6-BROMO-3-(4-BROMO-PHENYL)-3,4-DIHYDRO-2H-BENZO[E][1,3]OXAZINE 95.00%
5MG
$ 501.58

Total 4 raw suppliers

Chemical Property of 6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine

Chemical Property:

Vapor Pressure:8.44E-09mmHg at 25°C
Boiling Point:464.3oC at 760 mmHg
Flash Point:234.6oC
PSA：12.47000
Density:1.717g/cm3
LogP:4.63310
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:368.91869
Heavy Atom Count:18
Complexity:281

Purity/Quality:

95% ^*data from raw suppliers

6-BROMO-3-(4-BROMO-PHENYL)-3,4-DIHYDRO-2H-BENZO[E][1,3]OXAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=C(C=CC(=C2)Br)OCN1C3=CC=C(C=C3)Br

Technology Process of 6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine

There total 5 articles about 6-bromo-3-(4-bromophenyl)-3,4-dihydro-2H-1,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93186-78-8
4-bromo-2-[(4-bromophenylimino)methyl]phenol

: 7331-80-8
6-bromo-3-(4-bromo-phenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 5 °C

2: KOH / methanol / 2 h / Heating

With potassium hydroxide; sodium tetrahydroborate; In methanol;
DOI:10.1002/jps.2600810721

Reference yield:

: 106-40-1
4-bromo-aniline

: 7331-80-8
6-bromo-3-(4-bromo-phenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0.5 h

2: NaBH₄ / methanol / 5 °C

3: KOH / methanol / 2 h / Heating

With potassium hydroxide; sodium tetrahydroborate; In methanol;
DOI:10.1002/jps.2600810721

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 7331-80-8
6-bromo-3-(4-bromo-phenyl)-3,4-dihydro-2H-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0.5 h

2: NaBH₄ / methanol / 5 °C

3: KOH / methanol / 2 h / Heating

With potassium hydroxide; sodium tetrahydroborate; In methanol;
DOI:10.1002/jps.2600810721