Technology Process of Decanenitrile, 4-oxo-
There total 1 articles about Decanenitrile, 4-oxo- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
at 80 ℃;
for 2h;
under 60800 Torr;
DOI:10.1021/jo00017a001
- Guidance literature:
-
Multi-step reaction with 2 steps
1: L-(-)-glucose; bakers’ yeast ketoreductase / aq. phosphate buffer / 28 °C / pH 7.4 / Enzymatic reaction
2: dmap; dicyclohexyl-carbodiimide
With
dmap; L-(-)-glucose; bakers’ yeast ketoreductase; dicyclohexyl-carbodiimide;
In
aq. phosphate buffer;
DOI:10.1055/s-0033-1339282
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: L-(-)-glucose; bakers’ yeast ketoreductase / aq. phosphate buffer / 28 °C / pH 7.4 / Enzymatic reaction
2.1: water; dihydrogen peroxide; sodium hydroxide / 2 h / 70 °C
2.2: pH 2 - 3
With
L-(-)-glucose; bakers’ yeast ketoreductase; water; dihydrogen peroxide; sodium hydroxide;
In
aq. phosphate buffer;
DOI:10.1055/s-0033-1339282