2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine

Base Information

Chemical Name:2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine
CAS No.:73671-44-0
Molecular Formula:C13H13NS
Molecular Weight:215.319
Hs Code.:

Synonyms:2-amino-2'-methylsulfanylbiphenyl;2-(1-METHYLIMIDAZOL-2-YL)-1H-BENZOIMIDAZOLE-5-CARBOXYLIC ACID;2'-methylsulfanyl-biphenyl-2-ylamine;2'-Amino-2'-methylthiobiphenyl;2-amino-2'-methylthiobiphenyl;

Suppliers and Price of 2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2'-(METHYLSULFANYL)[1,1'-BIPHENYL]-2-YLAMINE 95.00%
5MG
$ 498.66

Total 0 raw suppliers

Chemical Property of 2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine

Chemical Property:

PSA：51.32000
LogP:4.23890

Purity/Quality:: 2'-(METHYLSULFANYL)[1,1'-BIPHENYL]-2-YLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine

There total 8 articles about 2'-(methylsulfanyl)[1,1'-biphenyl]-2-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 615-36-1
2-bromoaniline

: 168618-42-6
(2-methylsulfanylphenyl)boronic acid

: 73671-44-0
2-(2′-(methylthio)phenyl)aniline

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In tetrahydrofuran; ethanol; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201606285

Reference yield: 47.9%

: 73671-43-9
2-methylthio-2'-nitrobiphenyl

: 73671-44-0
2-(2′-(methylthio)phenyl)aniline

Guidance literature:: With calcium chloride; zinc; In ethanol; for 6h; Heating;
DOI:10.1248/cpb.32.4360

Reference yield:

: 33775-94-9
2-(methylthio)iodobenzene

: 73671-44-0
2-(2′-(methylthio)phenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 51.3 percent / copper / 1.5 h / 200 °C

2: 47.9 percent / Zn, CaCl₂ / aq. ethanol / 6 h / Heating

With copper; calcium chloride; zinc; In ethanol;
DOI:10.1248/cpb.32.4360