9-(2-Azidophenyl)-9H-fluorene

Base Information

Chemical Name:9-(2-Azidophenyl)-9H-fluorene
CAS No.:74357-30-5
Molecular Formula:C19H13N3
Molecular Weight:283.32700
Hs Code.:
DSSTox Substance ID:DTXSID60530994
Nikkaji Number:J1.405.055H
Wikidata:Q82402508

Synonyms:9-(2-AZIDOPHENYL)-9H-FLUORENE;74357-30-5;2-(9-fluorenyl)-phenyl azide;DTXSID60530994

Suppliers and Price of 9-(2-Azidophenyl)-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(2-Azidophenyl)-9H-fluorene

Chemical Property:

PSA：49.75000
LogP:5.24176
XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:283.110947427
Heavy Atom Count:22
Complexity:420

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(C3=CC=CC=C32)C4=CC=CC=C4N=[N+]=[N-]

Technology Process of 9-(2-Azidophenyl)-9H-fluorene

There total 5 articles about 9-(2-Azidophenyl)-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(9H-Fluoren-9-yl)-benzenediazonium; chloride

: 74357-30-5
o-(9-fluorenyl)phenyl azide

Guidance literature:: With sodium azide; In water; at 40 - 50 ℃; for 0.166667h; Yield given;
DOI:10.1021/ja00342a036

Reference yield:

: 75819-53-3
o-(9-fluorenyl)aniline

: 74357-30-5
o-(9-fluorenyl)phenyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) gas HCl, 2.) sodium nitrite, conc. HCl / 1.) benzene, 2.) 0 - 5 deg C, 10 min

2: sodium azide / H₂O / 0.17 h / 40 - 50 °C

With hydrogenchloride; sodium azide; sodium nitrite; In water;
DOI:10.1021/ja00342a036

Reference yield:

: 31859-87-7
N-phenyl-9H-fluoren-9-amine

: 74357-30-5
o-(9-fluorenyl)phenyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / aluminum chloride / 11 h / 180 °C

2: 1.) gas HCl, 2.) sodium nitrite, conc. HCl / 1.) benzene, 2.) 0 - 5 deg C, 10 min

3: sodium azide / H₂O / 0.17 h / 40 - 50 °C

With hydrogenchloride; aluminium trichloride; sodium azide; sodium nitrite; In water;
DOI:10.1021/ja00342a036