2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one

Base Information

Chemical Name:2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one
CAS No.:74457-12-8
Molecular Formula:C9H16O2Se
Molecular Weight:235.185
Hs Code.:
DSSTox Substance ID:DTXSID10502161

Synonyms:74457-12-8;2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one;DTXSID10502161

Suppliers and Price of 2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:236.03155
Heavy Atom Count:12
Complexity:170

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C1C(CCCC1=O)[Se]C)O

Technology Process of 2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one

There total 1 articles about 2-(1-Hydroxyethyl)-3-(methylselanyl)cyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-68-7
cyclohexenone

: 75-24-1
trimethylaluminum

: 75-07-0,9002-91-9
acetaldehyde

: 74457-12-8
2-(1-hydroxyethyl)-3-(methylseleno)cyclohexanone

Guidance literature:: With selenium; Yield given. Multistep reaction;
DOI:10.1246/bcsj.54.274

Reference yield: 77.0%

: 74457-12-8
2-(1-hydroxyethyl)-3-(methylseleno)cyclohexanone

: 67720-34-7
2-(1-hydroxyethyl)-2-cyclohexen-1-one

Guidance literature:: With pyridine; dihydrogen peroxide; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1246/bcsj.54.274

Reference yield:

: 74457-12-8
2-(1-hydroxyethyl)-3-(methylseleno)cyclohexanone

: 59697-64-2
(E)-2-ethylidene-3-methylcyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / pyridine, 30percent H₂O₂ / CH₂Cl₂ / 0.5 h / 25 °C

2: pyridine

3: 59 percent / diethyl ether / a) -23 deg C, 17 min, b) 0 deg C, 5 min

With pyridine; dihydrogen peroxide; In diethyl ether; dichloromethane;
DOI:10.1246/bcsj.54.274