1H-Pyrrole-3-propanoic acid, 5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4- methyl-, methyl ester

Base Information

Chemical Name:1H-Pyrrole-3-propanoic acid, 5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4- methyl-, methyl ester
CAS No.:74839-17-1
Molecular Formula:C34H42N2O10
Molecular Weight:638.715
Hs Code.:

1H-Pyrrole-3-propanoic acid,
5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth
oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4-
methyl-, methyl ester

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Chemical Property of 1H-Pyrrole-3-propanoic acid, 5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4- methyl-, methyl ester

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Technology Process of 1H-Pyrrole-3-propanoic acid, 5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4- methyl-, methyl ester

There total 9 articles about 1H-Pyrrole-3-propanoic acid, 5-[(1,1-dimethylethoxy)carbonyl]-2-[[3-(2-methoxy-2-oxoethyl)-4-(3-meth oxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-1H-pyrrol-2-yl]methyl]-4- methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 51644-18-9
2-tert-(Butoxycarbonyl)-4-(2-(methoxycarbonyl)ethyl)-3-methylpyrrole

: 50622-67-8
5-acetoxymethyl-3-(2-methoxycarbonyl-ethyl)-4-methoxycarbonylmethyl-pyrrole-2-carboxylic acid benzyl ester

: 74839-17-1
t-butyl 5'-benzyloxycarbonyl-3,4'-bis(2-methoxycarbonylethyl)-3'-methoxycarbonylmethyl-4-methylpyrromethane-5-carboxylate

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid; at 45 ℃; for 3h;
DOI:10.1039/P19870000277

Reference yield:

: 60204-91-3
t-butyl 5-iodo-4-(2-methoxycarbonylethyl)-3-methylpyrrole-2-carboxylate

: 74839-17-1
t-butyl 5'-benzyloxycarbonyl-3,4'-bis(2-methoxycarbonylethyl)-3'-methoxycarbonylmethyl-4-methylpyrromethane-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / anhyd. sodium acetate,, H₂ / platinum oxide / ethanol / 4 h / 20 °C / 760 Torr

2: 76 percent / p-TsOH*H₂O / acetic acid / 3 h / 45 °C

With hydrogen; sodium acetate; toluene-4-sulfonic acid; platinum(IV) oxide; In ethanol; acetic acid;
DOI:10.1039/P19870000277

Reference yield:

: 39265-95-7
methyl 3-acetyl-4-oxopentanoate

: 74839-17-1
t-butyl 5'-benzyloxycarbonyl-3,4'-bis(2-methoxycarbonylethyl)-3'-methoxycarbonylmethyl-4-methylpyrromethane-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CCl₄, Mg / 1.) ethanol, reflux, 6 h; 2.) reflux, 3 h, 5 deg C

2: 16 percent

4: 76 percent / p-TsOH*H₂O / acetic acid / 3 h / 45 °C

With tetrachloromethane; toluene-4-sulfonic acid; magnesium; In acetic acid;
DOI:10.1039/P19870000277