4,5-Diiodobenzene-1,2-diamine

Base Information

Chemical Name:4,5-Diiodobenzene-1,2-diamine
CAS No.:76179-43-6
Molecular Formula:C6H6I2N2
Molecular Weight:359.936
Hs Code.:
European Community (EC) Number:809-627-1
DSSTox Substance ID:DTXSID30469429
Wikidata:Q82297150
Mol file:76179-43-6.mol

Synonyms:4,5-diiodobenzene-1,2-diamine;76179-43-6;4,5-DIIODO-BENZENE-1,2-DIAMINE;C6H6I2N2;4,5-di-iodo-o-phenylenediamine;SCHEMBL240998;4,5-diiodo-o-phenylenediamine;1,2-Diamino-4,5-diiodobenzene;DTXSID30469429;DIBFUNSINNCILZ-UHFFFAOYSA-N;BDA17943;MFCD08458309;AKOS015964736;SB38632;AS-59893;CS-0342694;4,5-Diiodo-benzene-1,2-diamine, AldrichCPR;W18968

Suppliers and Price of 4,5-Diiodobenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

J&W Pharmlab
4,5-Diiodo-benzene-1,2-diamine 97%
1g
$ 398.00

J&W Pharmlab
4,5-Diiodo-benzene-1,2-diamine 97%
5g
$ 1390.00

Crysdot
4,5-Diiodobenzene-1,2-diamine 95+%
1g
$ 402.00

American Custom Chemicals Corporation
4,5-DIIODO-BENZENE-1,2-DIAMINE 95.00%
5MG
$ 504.54

Alichem
4,5-Diiodobenzene-1,2-diamine
1g
$ 328.00

Total 7 raw suppliers

Chemical Property of 4,5-Diiodobenzene-1,2-diamine

Chemical Property:

Melting Point:135-136 °C(Solv: ethanol (64-17-5); water (7732-18-5))
Boiling Point:397.2±42.0 °C(Predicted)
PKA:2.70±0.10(Predicted)
PSA：52.04000
Density:2.605±0.06 g/cm3(Predicted)
LogP:3.22260
XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:359.86204
Heavy Atom Count:10
Complexity:106

Purity/Quality:

97% ^*data from raw suppliers

4,5-Diiodo-benzene-1,2-diamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CC(=C1I)I)N)N

Technology Process of 4,5-Diiodobenzene-1,2-diamine

There total 3 articles about 4,5-Diiodobenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 29270-47-1
1,2-diiodo-4,5-dinitrobenzene

: 76179-43-6
4,5-di-iodo-o-phenylenediamine

Guidance literature:: With hydrogenchloride; tin(II) chloride dihdyrate; at 60 ℃; for 24h; Cooling with ice;
DOI:10.3390/molecules26113163

Reference yield:

: 29270-48-2
2-nitro-4,5-di-iodoaniline

: 76179-43-6
4,5-di-iodo-o-phenylenediamine

Guidance literature:: With hydrogenchloride; sodium hydroxide; stannous chloride; In water;

Reference yield:

: 528-29-0
1,2-Dinitrobenzene

: 76179-43-6
4,5-di-iodo-o-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / I₂; oleum / 1.25 h / 120 °C

2: 66 percent / Fe; aq. HCl / ethanol / 0.75 h / Heating

With hydrogenchloride; sulfuric acid; iodine; iron; In ethanol;
DOI:10.1021/jo052122l