Aluminum, chlorobis(trimethylsilyl)-

Base Information

Chemical Name:Aluminum, chlorobis(trimethylsilyl)-
CAS No.:77944-77-5
Molecular Formula:C6H18AlClSi2
Molecular Weight:208.814
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Aluminum, chlorobis(trimethylsilyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Aluminum, chlorobis(trimethylsilyl)-

There total 2 articles about Aluminum, chlorobis(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Al(SiMe₃)3*OEt₂

: 84174-75-4
ClPhPN(SiMe₃)2

: 75-77-4
chloro-trimethyl-silane

: 77944-77-5
bis(trimethylsilyl)aluminium chloride

: 118318-99-3
(C₆H₅){(CH₃)3Si}2NPP{(CH₃)3Si}2N(C₆H₅)

: 60-29-7,927820-24-4
diethyl ether

Guidance literature:: In hexane; combining (Me3Si)3Al.Et2O-soln. with Ph2PN(SiMe3)2-soln. at -78 °C, warming to 25 °C and stirring for 4 h ; under inert gas; evapn., (31P)-NMR, IR and MS;

Reference yield:

: Al(SiMe₃)3*OEt₂

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 75-77-4
chloro-trimethyl-silane

: 77944-77-5
bis(trimethylsilyl)aluminium chloride

: 60-29-7,927820-24-4
diethyl ether

: 1101-41-3
Tetraphenyldiphosphin

Guidance literature:: In toluene; combining (Me3Si)3Al.Et2O-soln. with Ph2PCl-soln. at -78 °C, stirring and warming to 25 °C overnight ; under inert gas; evapn., (31P)-NMR, IR and MS;