1-(2-phenylhydrazinyl)hexose

Base Information

• Chemical Name: 1-(2-phenylhydrazinyl)hexose
• CAS No.: 24758-68-7
• Molecular Formula: C₁₂H₁₈N₂O₆
• Molecular Weight: 286.285
• Mol file: 24758-68-7.mol

Synonyms:Gluconicacid, 2-phenylhydrazide, D- (8CI); 1-D-Glucono-2-phenylhydrazide; D-Gluconicacid phenylhydrazide; NSC 226832

Chemical Property of 1-(2-phenylhydrazinyl)hexose

Chemical Property:

• Vapor Pressure: 5.63E-15mmHg at 25°C
• Boiling Point: 594.4°Cat760mmHg
• Flash Point: 313.3°C
• Density: 1.535g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-phenylhydrazinyl)hexose

There total 9 articles about 1-(2-phenylhydrazinyl)hexose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-galactonic acid (133-42-6,488-33-5,526-95-4,526-97-6,576-36-3,642-99-9,1114-17-6,3956-93-2,6906-37-2,7760-07-8,13382-27-9,20246-33-7,20246-35-9,20246-52-0,20246-53-1,21675-42-3,22430-69-9,24871-35-0,28223-42-9,51547-37-6,28278-17-3) → L-talonic acid-(N'-phenyl-hydrazide) (6294-74-2,24758-68-7,29617-77-4,92998-70-4,136981-91-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; water

2: aqueous acetic acid

With pyridine; water; acetic acid;

Reference yield:

gluconic acid (526-95-4) → phenylhydrazide of D-gluconic acid (24758-68-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / aq. HCl / 0.02 h / microwave irradiation

2: hydrazine hydrate / ethanol / 0.01 h / microwave irradiation

With hydrogenchloride; hydrazine hydrate; In ethanol;

DOI:10.1080/07328300701540258

Reference yield:

L-altronic acid (906366-08-3) + phenylhydrazine (100-63-0) → L-altronic acid-(N'-phenyl-hydrazide) (6294-74-2,24758-68-7,29617-77-4,92998-70-4,136981-91-4)

Guidance literature:

DOI:10.1021/ja01303a036

upstream raw materials:

gluconic acid

phenylhydrazine

ethyl D-mannonate

D-Glucono-1,5-lactone