2-Azidophenyl disulfide

Base Information

Chemical Name:2-Azidophenyl disulfide
CAS No.:78715-74-9
Molecular Formula:C12H8N6S2
Molecular Weight:300.368
Hs Code.:
DSSTox Substance ID:DTXSID70508467
Wikidata:Q82365410
Mol file:78715-74-9.mol

Synonyms:2-Azidophenyl disulfide;78715-74-9;1-azido-2-[(2-azidophenyl)disulfanyl]benzene;dithiobisphenylazide;DTXSID70508467;1,1'-Disulfanediylbis(2-azidobenzene);FT-0720106

Suppliers and Price of 2-Azidophenyl disulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Azidophenyl disulfide

Chemical Property:

PSA：150.10000
LogP:5.27512
XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:300.02518663
Heavy Atom Count:20
Complexity:367

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)N=[N+]=[N-])SSC2=CC=CC=C2N=[N+]=[N-]

Technology Process of 2-Azidophenyl disulfide

There total 3 articles about 2-Azidophenyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1005-07-8
o-azidoaniline

: 67-64-1
acetone

: 23385-34-4
1-(benzothiazol-2-ylthio)propan-2-one

: 54467-95-7
1-azido-2-iodo-benzene

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 78715-74-9
bis(2-azidophenyl) disulfide

Guidance literature:: With sodium iodide; Product distribution; multistep reaction, other azidoaniline;
DOI:10.1021/jo00335a052

Reference yield:

: 1005-07-8
o-azidoaniline

: 23385-34-4
1-(benzothiazol-2-ylthio)propan-2-one

: 54467-95-7
1-azido-2-iodo-benzene

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 78715-74-9
bis(2-azidophenyl) disulfide

Guidance literature:: With hydrogenchloride; tetrafluoroboric acid; sodium iodide; sodium nitrite; Yield given. Multistep reaction. Yields of byproduct given; 1) H₂O, 0 deg C, 30 min, 2) acetone, CS₂, room temperature, 1-2 h;
DOI:10.1021/jo00335a052

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 1005-07-8
o-azidoaniline

: 23385-34-4
1-(benzothiazol-2-ylthio)propan-2-one

: 54467-95-7
1-azido-2-iodo-benzene

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 78715-74-9
bis(2-azidophenyl) disulfide

Guidance literature:: With hydrogenchloride; tetrafluoroboric acid; sodium iodide; sodium nitrite; Yield given. Multistep reaction. Yields of byproduct given; 1) H₂O, 0 deg C, 30 min, 2) acetone, room temperature, 1-2 h;
DOI:10.1021/jo00335a052