METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE

Base Information

Chemical Name:METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE
CAS No.:78775-33-4
Molecular Formula:C₁₀H₁₂ClNO₃
Molecular Weight:229.663
Hs Code.:
Mol file:78775-33-4.mol

Synonyms:methyl 5-chloro-2-methoxy-4-methylaminobenzoate;METHYL-5-CHLORO-2-METHOXY-4-N-METHYL AMINO BENZOATE;methyl 5-chloro-4-methylamino-2-methoxybenzoate;

Suppliers and Price of METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Alichem
Methyl5-chloro-2-methoxy-4-(methylamino)benzoate
10g
$ 2436.12

Total 7 raw suppliers

Chemical Property of METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE

Chemical Property:

PSA：47.56000
LogP:2.24990

Purity/Quality:

95% ^*data from raw suppliers

Methyl5-chloro-2-methoxy-4-(methylamino)benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE

There total 7 articles about METHYL 5-CHLORO-2-METHOXY-4-METHYLAMINOBENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 20896-27-9
methyl 4-amino-5-chloro-2-methoxybenzoate

: 78775-33-4
5-chloro-2-methoxy-4-(methylamino)benzoic acid methyl ester

: methyl 8-chloro-3-<2-chloro-5-methoxy-4-(methoxycarbonyl)phenyl>3,4-dihydro-5-methoxy-6-quinazolinecarboxylate

Guidance literature:: With hydrogenchloride; In ethanol; for 2.5h; Ambient temperature;
DOI:10.1016/S0040-4039(00)91955-5

Reference yield:

: 78775-32-3
methyl 5-chloro-2-methoxy-4-(N-methyl-N-tosylamido)benzoate

: 78775-33-4
5-chloro-2-methoxy-4-(methylamino)benzoic acid methyl ester

Guidance literature:: With sulfuric acid; at 50 ℃;
DOI:10.1021/jm00142a019

Reference yield:

: 78784-42-6
methyl 2-methoxy-4-(N-methyl-N-tosylamido)benzoate

: 78775-33-4
5-chloro-2-methoxy-4-(methylamino)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / chlorine / CHCl₃ / 3 - 10 °C

2: concd. sulfuric acid / 50 °C

With sulfuric acid; chlorine; In chloroform;
DOI:10.1021/jm00142a019