Diethyl (1-methylcyclohexyl)propanedioate

Base Information

Chemical Name:Diethyl (1-methylcyclohexyl)propanedioate
CAS No.:78775-64-1
Molecular Formula:C14H24O4
Molecular Weight:256.342
Hs Code.:
DSSTox Substance ID:DTXSID30506449
Wikidata:Q82362184

Synonyms:78775-64-1;Diethyl (1-methylcyclohexyl)propanedioate;SCHEMBL7207337;DTXSID30506449

Suppliers and Price of Diethyl (1-methylcyclohexyl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Diethyl (1-methylcyclohexyl)propanedioate

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:256.16745924
Heavy Atom Count:18
Complexity:274

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C(=O)OCC)C1(CCCCC1)C

Technology Process of Diethyl (1-methylcyclohexyl)propanedioate

There total 7 articles about Diethyl (1-methylcyclohexyl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 917-64-6
methyl magnesium iodide

: 41589-43-9
cyclohexylidene malonic acid diethyl ester

: 78775-64-1
(1-Methylcyclohexyl)malonsaeure-diethylester

Guidance literature:: With copper(l) chloride; In diethyl ether; at 0 - 20 ℃; for 1.75h;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 78775-64-1
(1-Methylcyclohexyl)malonsaeure-diethylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: TiCl₄ / tetrahydrofuran; CCl₄ / 0 °C

1.2: pyridine / tetrahydrofuran / 0 - 20 °C

2.1: CuCl / diethyl ether / 0 - 20 °C

With titanium tetrachloride; copper(l) chloride; In tetrahydrofuran; tetrachloromethane; diethyl ether; 1.1: Knoevenagel reaction;
DOI:10.1021/jm049924d

Reference yield:

: 105-53-3
diethyl malonate

: 78775-64-1
(1-Methylcyclohexyl)malonsaeure-diethylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: TiCl₄ / tetrahydrofuran; CCl₄ / 0 °C

1.2: pyridine / tetrahydrofuran / 0 - 20 °C

2.1: CuCl / diethyl ether / 0 - 20 °C

With titanium tetrachloride; copper(l) chloride; In tetrahydrofuran; tetrachloromethane; diethyl ether; 1.1: Knoevenagel reaction;
DOI:10.1021/jm049924d