6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone

Base Information

Chemical Name:6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone
CAS No.:6501-95-7
Molecular Formula:C6H8N4O2S
Molecular Weight:200.2183
Hs Code.:
NSC Number:95849
DSSTox Substance ID:DTXSID00215354
Nikkaji Number:J2.928.397D
Wikidata:Q83091381
ChEMBL ID:CHEMBL2131054

Synonyms:6501-95-7;6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone;NSC95849;NSC 95849;MLS002695331;NCIOpen2_001858;CHEMBL2131054;DTXSID00215354;ZNIGBVHXVZODGC-UHFFFAOYSA-N;HMS3079M23;NSC-95849;SMR001561237;6-amino-1,3-dimethyl-5-nitroso-2-thioxo-pyrimidin-4-one;4(1H)-Pyrimidinone, 6-amino-2,3-dihydro-1,3-dimethyl-5-nitroso-2-thioxo-

Suppliers and Price of 6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone

Chemical Property:

Vapor Pressure:0.0201mmHg at 25°C
Boiling Point:251.8°Cat760mmHg
Flash Point:106.1°C
Density:1.59g/cm³
XLogP3:-0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:200.03679668
Heavy Atom Count:13
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=C(C(=O)N(C1=S)C)N=O)N

Technology Process of 6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone

There total 4 articles about 6-Amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydro-4(1H)-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3120-52-3
6-amino-N¹,N³-dimethyl-2-thioxopyrimidin-4-one

: 6501-95-7
6-amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; for 0.333333h;
DOI:10.1021/jm00046a022

Reference yield:

: 1027454-59-6
1-(2-Cyano-acetyl)-1,3-dimethyl-thiourea

: 6501-95-7
6-amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / methanol / 0.17 h

2: 96 percent / NaNO₂, aq. HCl / H₂O / 0.33 h

With hydrogenchloride; sodium hydroxide; sodium nitrite; In methanol; water;
DOI:10.1021/jm00046a022

Reference yield:

: 96-31-1
N,N'-Dimethylurea

: 372-09-8
cyanoacetic acid

: 6501-95-7
6-amino-1,3-dimethyl-5-nitroso-2-thioxo-2,3-dihydropyrimidin-4(1H)-one

Guidance literature:: N,N'-Dimethylurea; cyanoacetic acid; With acetic anhydride;

With acetic acid; sodium nitrite;
DOI:10.1016/j.ica.2010.11.009