Silane, (2,3,4,5-tetraphenyl-1H-germol-1-ylidene)bis[trimethyl-

Base Information

Chemical Name:Silane, (2,3,4,5-tetraphenyl-1H-germol-1-ylidene)bis[trimethyl-
CAS No.:79411-53-3
Molecular Formula:C34H38GeSi2
Molecular Weight:575.437
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, (2,3,4,5-tetraphenyl-1H-germol-1-ylidene)bis[trimethyl-

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Technology Process of Silane, (2,3,4,5-tetraphenyl-1H-germol-1-ylidene)bis[trimethyl-

There total 5 articles about Silane, (2,3,4,5-tetraphenyl-1H-germol-1-ylidene)bis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 2Li⁽¹⁺⁾*GeC₄(C₆H₅)4^(2-)=Li₂GeC₄(C₆H₅)4

: 79411-53-3
1,1-bis(trimethylsilyl)-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

Guidance literature:: In tetrahydrofuran; excess of Me3SiCl, cooling (0°C), warming (room temp.), stirring (2 h); evapn. (vac.), extraction (pentane), filtn., concn., cooling (-10°C);
DOI:10.1002/anie.199610021

Reference yield: 87.0%

: 75-77-4
chloro-trimethyl-silane

: 16059-00-0
1,1-dihydro-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

: 79411-53-3
1,1-bis(trimethylsilyl)-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; byproducts: n-butane, lithium chloride; stirring of components at -78°C in N2 atm.; warming to room temp., evapn., addition of benzene, evapn., recrystn. (hexane), elem anal.;
DOI:10.1016/S0022-328X(00)84612-4

Reference yield: 87.0%

: 75-77-4
chloro-trimethyl-silane

: 16030-09-4
1,1-dichloro-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

: 79411-53-3
1,1-bis(trimethylsilyl)-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

Guidance literature:: With magnesium; In tetrahydrofuran; soln. of 1,1-dichloro-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene inTHF and Me3SiCl added under Ar to iodine-activated magnesium; react. mi xt. stirred for 1 h; THF removed in vac.; residue dissolved in benzene and filtered; solvent evapd. and residue recrystd. from hexane;
DOI:10.1007/s11172-005-0124-8