Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis-

Base Information

Chemical Name:Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis-
CAS No.:27697-57-0
Molecular Formula:C23H32 O6
Molecular Weight:404.503
Hs Code.:
Mol file:27697-57-0.mol

Synonyms:Ethanol,2,2'-[isopropylidenebis(p-phenyleneoxyethyleneoxy)]di- (8CI); BA 4U

Suppliers and Price of Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis-

There total 2 articles about Ethanol,2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxy-2,1-ethanediyloxy)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 80-05-7
BPA

: 628-89-7
2-(2-Chloroethoxy)ethanol

: 27697-57-0,99280-30-5
2,2'-[propane-2,2-diylbis(benzene-4,1-diyloxyethane-2,1-diyloxy)]diethanol

Guidance literature:: BPA; With 18-crown-6 ether; potassium carbonate; In acetonitrile; for 1h; Reflux; Inert atmosphere;

2-(2-Chloroethoxy)ethanol; In acetonitrile; for 72h; Inert atmosphere; Reflux;
DOI:10.1039/c1dt10815h

Reference yield:

: 80-05-7
BPA

: 107-21-1
ethylene glycol

: 27697-57-0,99280-30-5
2,2'-[propane-2,2-diylbis(benzene-4,1-diyloxyethane-2,1-diyloxy)]diethanol

Guidance literature:: With urea; zinc(II) oxide; at 170 ℃; for 7h;

Reference yield: 82.0%

: 27697-57-0,99280-30-5
2,2'-[propane-2,2-diylbis(benzene-4,1-diyloxyethane-2,1-diyloxy)]diethanol

: 861114-31-0
1,1'-propane-2,2-diylbis{4-[2-(2-bromoethoxy)ethoxy]benzene}

Guidance literature:: 2,2'-[propane-2,2-diylbis(benzene-4,1-diyloxyethane-2,1-diyloxy)]diethanol; With methanesulfonyl chloride; triethylamine; In dichloromethane; at -2 - 0 ℃; for 4h;

With lithium bromide; In acetone; for 16h; Further stages.; Heating;
DOI:10.1002/hlca.200790145