Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride

Base Information

Chemical Name:Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride
CAS No.:804518-04-5
Molecular Formula:C32H35N3O4.ClH
Molecular Weight:562.109
Hs Code.:

Formamide,
N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen
yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride

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Chemical Property of Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride

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Technology Process of Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride

There total 5 articles about Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 652990-08-4
(R)-2-bromo-1-tert-butyldimethylsilyloxy-1-(3-formamido-4-benzyloxyphenyl)ethane

: 321709-19-7
2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethylamine

: 804518-04-5
(R)-N-(2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine monohydrochloride

Guidance literature:: 2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethylamine; With sodium hydroxide; In Isopropyl acetate; water; for 0.133333h;

(R)-2-bromo-1-tert-butyldimethylsilyloxy-1-(3-formamido-4-benzyloxyphenyl)ethane; With potassium carbonate; In N,N-dimethyl acetamide; Isopropyl acetate; at 90 ℃; for 17h;

With acetic acid; cesium fluoride; sodium chloride; more than 3 stages; Product distribution / selectivity;

Reference yield: 71.0%

: 652990-08-4
(R)-2-bromo-1-tert-butyldimethylsilyloxy-1-(3-formamido-4-benzyloxyphenyl)ethane

: 2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethylamine bis-hydrobromide

: 804518-04-5
(R)-N-(2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine monohydrochloride

Guidance literature:: (R)-2-bromo-1-tert-butyldimethylsilyloxy-1-(3-formamido-4-benzyloxyphenyl)ethane; 2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethylamine bis-hydrobromide; With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 110 - 115 ℃; for 5h;

With acetic acid; cesium fluoride; In methanol; pentan-1-ol; at 55 ℃; for 4h;

With potassium carbonate; acetic acid; sodium chloride; more than 3 stages; Product distribution / selectivity;

Reference yield: 69.0%

: 2-bromo-(R)-1-tert-butyldimethylsiloxy-1-(3-formamido-4-benzyloxyphenyl)ethane

: 804518-04-5
(R)-N-(2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine monohydrochloride

Guidance literature:: N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine; With hydrogenchloride; In 1,4-dioxane; isopropyl alcohol; at 20 ℃;

2-bromo-(R)-1-tert-butyldimethylsiloxy-1-(3-formamido-4-benzyloxyphenyl)ethane; With potassium carbonate; In ISOPROPYLAMIDE; at 50 - 90 ℃; for 17h;

With cesium fluoride; In methanol; butanone; at 30 - 37 ℃; for 7.5h;