1H-Imidazolium, 1-(phenylmethyl)-3-(2-pyridinylmethyl)-, iodide

Base Information

Chemical Name:1H-Imidazolium, 1-(phenylmethyl)-3-(2-pyridinylmethyl)-, iodide
CAS No.:812644-47-6
Molecular Formula:C16H16N3.I
Molecular Weight:377.228
Hs Code.:

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Chemical Property of 1H-Imidazolium, 1-(phenylmethyl)-3-(2-pyridinylmethyl)-, iodide

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Technology Process of 1H-Imidazolium, 1-(phenylmethyl)-3-(2-pyridinylmethyl)-, iodide

There total 1 articles about 1H-Imidazolium, 1-(phenylmethyl)-3-(2-pyridinylmethyl)-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 4377-33-7
2-chloromethylpyridine

: 4238-71-5
1-benzylimidazole

: 812644-47-6
3-benzyl-1-(2-picolyl)imidazolium iodide

Guidance literature:: With sodium iodide; In acetone; for 48h;
DOI:10.1016/j.jorganchem.2005.03.015

Reference yield: 80.0%

: 812644-47-6
3-benzyl-1-(2-picolyl)imidazolium iodide

: 83864-14-6
nickel dichloride

: [Ni(3-benzyl-1-picolyimidazolium)Cl_2.5I_0.5]

Guidance literature:: In dimethyl sulfoxide; (Ar); std. Schlenk technique; soln. of NiCl2 and iodide in DMSO was stirredat 140°C for 2 d; DMSO removed in vac. at 50°C; recrystd. (MeOH/Et2O); elem. anal.;
DOI:10.1016/j.jorganchem.2005.03.015

Reference yield: 65.0%

: 812644-47-6
3-benzyl-1-(2-picolyl)imidazolium iodide

: dicarbonyldichlororuthenium

: trans(Cl)-dicarbonyldichloro[3-benzyl-1-(2-picolyl)imidazol-2-ylidene]ruthenium(II)

: cis(Cl)-dicarbonyldichloro[3-benzyl-1-(2-picolyl)imidazol-2-ylidene]ruthenium(II)

Guidance literature:: With Ag₂O; In dichloromethane; byproducts: AgBr; under N2; mixt. of imidazolium salt, Ag2O and CH2Cl2 stirred at room temp. for 12 h; filtered through Celite; Ru complex added to filtrate; stirred at room temp. for 12 h; filtered through Celite; sepd. by chromy. (silica gel, CH2Cl2-MeOH 40:1,CH2Cl2-MeOH 20:1); volatiles removed under vac.; elem. anal.;
DOI:10.1039/b904882k