Cobalt, tetracarbonyl(1-oxo-2-phenylpropyl)-

Base Information

Chemical Name:Cobalt, tetracarbonyl(1-oxo-2-phenylpropyl)-
CAS No.:82182-04-5
Molecular Formula:C13H9CoO5
Molecular Weight:304.205
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cobalt, tetracarbonyl(1-oxo-2-phenylpropyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Cobalt, tetracarbonyl(1-oxo-2-phenylpropyl)-

There total 4 articles about Cobalt, tetracarbonyl(1-oxo-2-phenylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 64519-62-6,16842-03-8
cobalt tetracarbonyl hydride

: 3156-07-8
methyl phenyl ketene

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 82182-04-5
2-phenylpropanoylcobalt tetracarbonyl

Guidance literature:: In ethanol; pentane; byproducts: α-phenylpropionaldehyde, ethylbenzene, styrene; a soln. of 2.0mmol HCo(CO)4 (preapred from Co2(CO)8, DMF and concd. HCl) in 2.5ml pentane and a soln. of 2.0mmol of the ketene in 5.5ml ether and 30μl cumene were reacted under 120bar CO at 10°C for 4d; mechanism discussed;; filtration of Co2(CO)8, investigation of soln. by IR showed presence ofCo-compound, gas-chromatography of soln. after quenching with methanol;further by-product: methyl α-phenylpropionate;;
DOI:10.1016/0022-328X(86)80136-X

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 64519-62-6,16842-03-8
cobalt tetracarbonyl hydride

: 82182-04-5
2-phenylpropanoylcobalt tetracarbonyl

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: C₆H₅CH(CH₃)Co(CO)4

: 100-41-4,27536-89-6
ethylbenzene

Guidance literature:: With carbon monoxide; In n-heptane; Heptane soln. in the presence of CO, 15°C; not sepd., detected by IR spectra and gas chromy.;; Kinetics;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 16972-33-1
pentacarbonylhydridomanganese

: 82182-04-5
2-phenylpropanoylcobalt tetracarbonyl

Guidance literature:: With carbon monoxide; In n-heptane; stock soln. added under CO to mixt. of Co2(CO)8 and styrene (35°C), gas uptake ratio measured after 5 min and 20 min; identification by IR;
DOI:10.1021/om00110a008