1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene

Base Information

Chemical Name:1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene
CAS No.:35088-71-2
Molecular Formula:C21H20 O2 S
Molecular Weight:336.4473
Hs Code.:
NSC Number:157934
DSSTox Substance ID:DTXSID30956521
Wikidata:Q82936604
Mol file:35088-71-2.mol

Synonyms:35088-71-2;NSC157934;DTXSID30956521;NSC-157934;1,1'-[(Phenylsulfanyl)methylene]bis(4-methoxybenzene)

Suppliers and Price of 1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene

Chemical Property:

Boiling Point:482.4°Cat760mmHg
Flash Point:245.6°C
Density:1.18g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:336.11840105
Heavy Atom Count:24
Complexity:316

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(C2=CC=C(C=C2)OC)SC3=CC=CC=C3

Technology Process of 1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene

There total 8 articles about 1-Methoxy-4-[(4-methoxyphenyl)-phenylsulfanylmethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (bis(4-methoxyphenyl)methyl)triphenylphosphonium trifluoromethanesulfonate

: 108-98-5
thiophenol

: 35088-71-2
(bis(4-methoxyphenyl)methyl)(phenyl)sulfane

Guidance literature:: In dimethyl sulfoxide; at 60 ℃; chemoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.202111164

Reference yield:

: 100-66-3
methoxybenzene

: 35088-71-2
(bis(4-methoxyphenyl)methyl)(phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 0.05 h / Inert atmosphere; Sealed tube

1.2: 24 h / 45 °C / Inert atmosphere; Sealed tube

2.1: dimethyl sulfoxide / 60 °C / Inert atmosphere; Sealed tube

In dimethyl sulfoxide; acetonitrile; 1.1: |Friedel-Crafts Alkylation / 1.2: |Friedel-Crafts Alkylation;
DOI:10.1002/anie.202111164

Reference yield:

: (hydroxy(4-methoxyphenyl)methyl)triphenylphosphonium trifluoromethanesulfonate

: 35088-71-2
(bis(4-methoxyphenyl)methyl)(phenyl)sulfane

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 45 °C / Inert atmosphere; Sealed tube

2: dimethyl sulfoxide / 60 °C / Inert atmosphere; Sealed tube

In dimethyl sulfoxide; acetonitrile;
DOI:10.1002/anie.202111164