Arsine, diphenyl[(tributylstannyl)methyl]-

Base Information

Chemical Name:Arsine, diphenyl[(tributylstannyl)methyl]-
CAS No.:82758-96-1
Molecular Formula:C25H39AsSn
Molecular Weight:533.216
Hs Code.:

Synonyms:

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Chemical Property of Arsine, diphenyl[(tributylstannyl)methyl]-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Arsine, diphenyl[(tributylstannyl)methyl]-

There total 3 articles about Arsine, diphenyl[(tributylstannyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1461-22-9
tributyltin chloride

: 61024-98-4
(diphenylarsano)methyl lithium

: 82758-96-1
diphenyl<(tributylstannyl)methyl>arsane

Guidance literature:: With water; In tetrahydrofuran; addn. of ClSnBu3 to a soln. of Ph2AsCH2Li in THF under N2; hydrolysis with H2O;; extn. with CHCl3 two times; drying of the extract over Na2SO4; column chromy. (Al2O3, benzine);;

Reference yield: 73.0%

: (tributylstannyl)methyl-lithium

: 712-48-1
chlorodiphenylarsine

: 82758-96-1
diphenyl<(tributylstannyl)methyl>arsane

Guidance literature:: With water; In diethyl ether; addn. of Ph2AsCl in ether to a soln. of LiCH2SnBu3 (prepd. by I/Li exchange with BuLi from Bu3SnCH2I) in ether at -50°C under N2; warming to room temp. (after 20 min); hydrolysis with H2O;; extn. with CHCl3 two times; drying of the extract over Na2SO4; evapn.; column chromy. of the oily residue (Al2O3, benzine); elem. anal.;;

Reference yield: 73.0%

: 712-48-1
chlorodiphenylarsine

: 66222-29-5
tri-n-butylstannylmethyl iodide

: 82758-96-1
diphenyl<(tributylstannyl)methyl>arsane

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; under N2 n-BuLi/hexane added at -50°C for 1 min, stirred for 8 min, ClAsPh2/ether added at -50°C, stirred for 20 min, allowed to room temp., hydrolysis with H2O; extd. (CHCl3), dried on Na2SO4, concd. in vac., chromy. (Al2O3, benzine), elem. anal.;