Arsine, pentyldiphenyl-

Base Information

• Chemical Name: Arsine, pentyldiphenyl-
• CAS No.: 38563-47-2
• Molecular Formula: C₁₇H₂₁As
• Molecular Weight: 300.275
• Mol file: 38563-47-2.mol

Synonyms:

Chemical Property of Arsine, pentyldiphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Arsine, pentyldiphenyl-

There total 8 articles about Arsine, pentyldiphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chlorodiphenylarsine (712-48-1) → Pentyldiphenylarsan (38563-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / PhLi / tetrahydrofuran; benzene; diethyl ether / 1.) -120 deg C, 2.) -120 deg C to r.t.

2: 1.) PhLi / 1.) THF, ether, benzene, -78 deg C, 30 min, 2.) THF, ether, benzene, -50 deg C to r.t., overnight

With phenyllithium; In tetrahydrofuran; diethyl ether; benzene;

Reference yield:

phenylhydrazine (100-63-0) → Pentyldiphenylarsan (38563-47-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) 80 percent arsenic acid, CuO, 2.) conc. HCl / 1.) H₂O, 70 deg C, 2 h, 2.) CCl₄, 5 min

2: 76 percent / PhLi / tetrahydrofuran; benzene; diethyl ether / 1.) -120 deg C, 2.) -120 deg C to r.t.

3: 1.) PhLi / 1.) THF, ether, benzene, -78 deg C, 30 min, 2.) THF, ether, benzene, -50 deg C to r.t., overnight

With hydrogenchloride; orthoarsenic acid; phenyllithium; copper(II) oxide; In tetrahydrofuran; diethyl ether; benzene;

Reference yield:

Pentyldiphenylarsanoxid (61025-00-1) → Pentyldiphenylarsan (38563-47-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

upstream raw materials:

Pentyldiphenylarsanoxid

1-bromo-butane

(diphenylarsino)methyl iodide

diphenyl<(tributylstannyl)methyl>arsane