3-(phenyliMino)pentane-2,4-dione

Base Information

Chemical Name:3-(phenyliMino)pentane-2,4-dione
CAS No.:83325-65-9
Molecular Formula:C11H11NO2
Molecular Weight:189.21100
Hs Code.:2914290090
Mol file:83325-65-9.mol

Synonyms:(phenylethyl)triphenylphosphonium bromide;2-(phenylhydrazono)propanedioyl dichloride;3-(phenylimino)pentane-2,4-dione;2-phenylhydrazonomalonyl dichloride;PhNHN=C(COCl)2;(phenylimino)acetylacetone;Phenylimino-acetylaceton;triphenyl(phenylethynyl)phosphonium bromide;triphenyl(phenylethynyl)phosphonium;(phenylethynyl)triphenylphosphonium bromide;(Phenylhydrazono-methyl)-malonsaeure-diaethylester;2-(2-phenylhydrazono)malonyl dichloride;(phenylhydrazono-methyl)-malonic acid diethyl ester;Formylmalonsaeure-diaethylester-phenylhydrazon;triphenyl-(2-phenylethynyl)phosphanium;(2-phenylethynyl)triphenylphosphonium bromide;N-<2.4-Dioxo-pentyliden-(3)>-anilin;mesoxaloyl dichloride phenylhydrazone;(phenylhydrazono)propandioyl dichloride;

Suppliers and Price of 3-(phenyliMino)pentane-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
3-(Phenylimino)pentane-2,4-dione
1g
$ 121.00

Apolloscientific
3-(Phenylimino)pentane-2,4-dione >98%
1g
$ 299.00

Total 7 raw suppliers

Chemical Property of 3-(phenyliMino)pentane-2,4-dione

Chemical Property:

PSA：46.50000
LogP:1.93710

Purity/Quality:

≥95% ^*data from raw suppliers

3-(Phenylimino)pentane-2,4-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(phenyliMino)pentane-2,4-dione

There total 2 articles about 3-(phenyliMino)pentane-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 586-96-9
Nitrosobenzene

: 123-54-6,81235-32-7
acetylacetone

: 83325-65-9
3-(phenylimino)pentane-2,4-dione

Guidance literature:: With 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((1S)-(6-methoxyquinolin-4-yl)((2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)amino)cyclobut-3-ene-1,2-dione; In chloroform; at 25 ℃; for 2h; Solvent; Molecular sieve;
DOI:10.1002/anie.201506206

Reference yield:

: 83325-65-9
3-(phenylimino)pentane-2,4-dione

Guidance literature:: Acetylaceton, Nitrosobenzol, A., Triaethylamin;
DOI:10.1246/bcsj.36.870

Reference yield: 94.0%

: C₁₆H₁₇NO₄

: 83325-65-9
3-(phenylimino)pentane-2,4-dione

: C₂₇H₂₈N₂O₆

Guidance literature:: With 3-((3,5-bis(trifluoromethyl)benzyl)amino)-4-(((1S)-(6-methoxyquinolin-4-yl)((2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)amino)cyclobut-3-ene-1,2-dione; In chloroform; at 25 ℃; for 48h; stereoselective reaction;
DOI:10.1002/anie.201506206